香熊猫茎活性炭的制备与表征

Q4 Biochemistry, Genetics and Molecular Biology
P. Dim, Augustine U. Iloka, J. Okafor
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引用次数: 0

摘要

以一种新的前体香椰茎为原料合成了活性炭。考察了氢氧化钠、NaOH、氯化锌、ZnCl2和磷酸、H3PO4等不同助剂对制备的吸附剂的影响。用化学试剂制备吸附剂,在400℃下碳化1小时。采用扫描电镜(SEM)、能量色散x射线(EDX)、x射线衍射(XRD)和傅里叶变换红外光谱(FTIR)对其表面形貌、元素组成和官能团进行了分析。图像分析表明,吸附剂中存在微孔和介孔。H3PO4活性炭的最大比表面积为2648 m2/g,孔隙体积为1.683 cm3/g,对碘和亚甲基蓝的最高吸附量分别为541和105 mg/g。熊猫枝干因其丰富、易获取、价格低廉、易得而成为制备高孔吸附剂的替代材料。关键词:活化,吸附,碘值,亚甲基蓝,烛台熊猫,试剂
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Preparation and Characterization of Activated Carbon from Pandanus candelabrum Stem
Pandanus candelabrum stem, a new precursor, was used to synthesise activate carbon. The effect of sodium hydroxide, NaOH, zinc (II) chloride, ZnCl2 and phosphoric acid, H3PO4, different agents on prepared adsorbents was investigated. The adsorbents were prepared with chemical agents and carbonized at 400 oC for 1 hour. Surface morphology, elemental composition and functional groups were analysed with scanning electron microscopy (SEM), energy dispersive X-ray (EDX), X-ray diffraction (XRD) and fourier transform infrared spectroscopy (FTIR), respectively. The image analysis showed the presence of both micropores and mesopores in the adsorbents. The H3PO4 activated carbon had the maximum surface area (2648 m2/g), pore volume (1.683 cm3/g) and highest adsorption for iodine and methylene blue were 541 and 105 mg/g. Pandanus candelabrum stem is an alternative material that can be used to synthesis high porous adsorbent because is abundant, easy to access, inexpensive and readily available.   Keywords: Activated, adsorption, iodine number, methylene blue, Pandanus candelabrum, reagents
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来源期刊
Borneo Journal of Resource Science and Technology
Borneo Journal of Resource Science and Technology Agricultural and Biological Sciences-Forestry
CiteScore
0.70
自引率
0.00%
发文量
16
审稿时长
12 weeks
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