γ辐照法制备纳米银/CM壳聚糖-异丙醇的绿色合成与表征

IF 1 Q4 MATERIALS SCIENCE, COMPOSITES
S. J. Beden, A. A. Ati, Kifah A. Fayadh Alimarah, Suhailah K Saihood, Rana K. Abdulnabi, M. Mejbel
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引用次数: 2

摘要

本研究证明了使用伽马辐射条件合成球形稳定的银纳米颗粒Ag NPs的绿色工艺。与传统方法相比,该方法具有一定的优势,因为它可以控制颗粒大小和结构,并产生完全还原的、极纯的、不含副产物或化学还原剂的纳米颗粒。银纳米粒子复合物(Ag-NPs/CM)是由硝酸银、壳聚糖和异丙醇的水溶液在室温下制备的,使用γ辐照剂量诱导还原和交联以原位形成Ag-NPs-CM壳聚糖异丙醇溶液。使用透射电子显微镜、XRD、Zeta电位和UV-Vis分光光度计分析表征了银纳米颗粒在水凝胶基质中的产生和均匀分布。银/CM壳聚糖异丙醇基质在Co-60γ源下具有不同的γ剂量。通过对IR-Ag NPs/(CM-壳聚糖异丙醇溶液进行抗菌活性测试的综合结果表明,制备的Ag NPs/CM-壳聚糖-异丙醇溶液可作为抗菌剂使用。所得Ag纳米粒子在室温下稳定3个月以上(CM壳聚糖-异丙醇)在未来的抗菌应用中具有很好的应用前景。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Green Synthesis and Characterization of Silver Nanoparticles / CM-Chitosan-Isopropanol by Gamma Irradiations Method
The present study demonstrates a green process for the synthesis of spherical-shaped and stabilized silver nanoparticles Ag NPs using gamma irradiated conditions. This method has certain advantages over conventional methods since it can manage the particle size and structure and generates totally reduced and extremely pure nanoparticles free from by-products or chemical reducing agents. Silver nanoparticles composite (Ag NPs / CM) is prepared from an aqueous solution of silver nitrate, chitosan and isopropanol, at room temperature using gamma irradiation doses to induce reduction and cross-linking to formation in situ Ag NPs/ CM-chitosan-isopropanol solutions. The production and homogenous distribution of silver nanoparticles in the hydrogel matrix were characterized using transmission electron microscopy, XRD, Zeta potential and UV-Vis spectrophotometer analysis. The silver/ CM-chitosan-isopropanol matrixes possessed different gamma doses using a Co- 60 gamma source. Through the comprehensive results of IR- Ag NPs /(CM- chitosan isopropanol solutions due to antibacterial activity test, the results show the prepared Ag NPs /CM-chitosan-isopropanol could be used as an antibacterial agent. The obtained Ag nanoparticles were stable for over 3 months at room temperature. the analysis outcomes indicate that the colloidal Solution (silver nanoparticles / (CM chitosan - isopropanol)) has a promising ability to be used in antibacterial applications in the future.
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来源期刊
CiteScore
1.90
自引率
25.00%
发文量
32
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