2-（（（2,7-二羟基萘-1-基）亚甲基）氨基-3'，6'-双（乙基氨基）-2'，7'-二甲基螺[异吲哚啉-1,9'-黄嘌呤]-3-酮的合成、表征及水中铀的比色检测。

IF 0.6 Q4 CHEMISTRY, ORGANIC

Molbank Pub Date : 2023-09-01 Epub Date: 2023-09-15 DOI:10.3390/m1725

Rahisa Mohammed, Peace Ogadi, Dennis M Seth, Amrutaa Vibho, Sarah K Gallant, Rory Waterman

引用次数: 0

摘要

以罗丹明6G酰肼（采用文献方法制备）和市售的2,7-二羟基萘-1-甲醛为原料，通过亚胺缩合反应合成了2-（（（2,7-二羟萘-1-基）亚甲基）氨基-3'，6'-双（乙基氨基）-2'，7'-二甲基螺[异吲哚啉-1,9'-黄嘌呤]-3-酮。使用FT-IR、1H-NMR、13C-NMR、X射线和HRMS进行结构表征。这种希夫碱有望成为水中铀比色分析的配体。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

Synthesis and Characterization of 2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3',6'-bis(ethylamino)-2',7'-dimethylspiro[isoindoline-1,9'-xanthen]-3-one and Colorimetric Detection of Uranium in Water.

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2-(((2,7-Dihydroxynaphthalen-1-yl)methylene)amino)-3',6'-bis(ethylamino)-2',7'-dimethyl-spiro[isoindoline-1,9'-xanthen]-3-one was synthesized using Rhodamine 6G hydrazide (prepared using literature methods) and commercially available 2,7-dihydroxynaphthalene-1-carbaldehyde via imine condensation. Structural characterization was performed using FT-IR, ¹H-NMR, ¹³C-NMR, X-ray, and HRMS. This Schiff base shows promise as a ligand for the colorimetric analysis of uranium in water.

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来源期刊

Molbank Chemistry-Physical and Theoretical Chemistry

CiteScore

0.70

自引率

33.30%

发文量

174

审稿时长

11 weeks

期刊介绍： •organic synthesis •biosynthesis •extraction and purification •natural product derivatives •structural elucidation (X-ray crystallography, NMR, etc.)