苯乙二醛衍生物合成的新方法

IF 0.8 4区化学 Q4 CHEMISTRY, MULTIDISCIPLINARY

Doklady Chemistry Pub Date : 2022-11-02 DOI:10.1134/S0012500822600109

Yu. V. Myasoedova, G. N. Sakhabutdinova, E. R. Belyaeva, G. Z. Raskil’dina, G. Yu. Ishmuratov, S. S. Zlotsky

引用次数: 0

摘要

本文提出了一种以苯丙烯醛缩醛为原料的一锅臭氧分解合成酰基腙的新方法，该方法包括在甲醇中臭氧分解底物，并用过量的癸酸、烟酸、异烟酸、苯甲酸和对羟基苯甲酸的肼处理中间过氧化物。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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New Method for the Synthesis of Phenylglyoxal Derivatives

The paper proposes a new one-pot ozonolytic synthesis of acylhydrazones from phenylacrolein acetals, which includes ozonolytic cleavage of the substrate in methanol and treatment of the intermediate peroxides with hydrazides of capric, nicotinic, isonicotinic, benzoic, and para-hydroxybenzoic acids taken in excess.

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来源期刊

Doklady Chemistry 化学-化学综合

CiteScore

1.20

自引率

12.50%

发文量

审稿时长

6-12 weeks

期刊介绍： Doklady Chemistry is a journal that publishes new research in chemistry and chemical engineering of great significance. Initially the journal was a forum of the Russian Academy of Science and published only best contributions from Russia in the form of short articles. Now the journal welcomes submissions from any country in the English or Russian language. Every manuscript must be recommended by Russian or foreign members of the Russian Academy of Sciences.