Lyudmila G Kuz'mina, Ivan I Konstantinov, Andrei V Churakov, Mger A Navasardyan
{"title":"4-[(3-甲基-但3-烯基)-氧]苯基4-正己基氧苯甲酸酯的晶体结构。","authors":"Lyudmila G Kuz'mina, Ivan I Konstantinov, Andrei V Churakov, Mger A Navasardyan","doi":"10.1107/S2056989017008568","DOIUrl":null,"url":null,"abstract":"<p><p>The structure of the title compound, C<sub>23</sub>H<sub>26</sub>O<sub>5</sub> or CH<sub>2</sub>=C(CH<sub>3</sub>)-C(O)O-C<sub>6</sub>H<sub>4</sub>-O(O)C-C<sub>6</sub>H<sub>4</sub>-OC<sub>6</sub>H<sub>13</sub>, has been determined. The mol-ecule is non-planar and the dihedral angle between the phenyl rings is 50.72 (4)°. The crystal packing differs from those typical for mesogenic compounds. Only a weak directional inter-action of the C-H⋯O type combines mol-ecules in endless chains running along the <i>a</i> axis.</p>","PeriodicalId":7015,"journal":{"name":"Acta Crystallographica Section E Crystallographic Communications","volume":" ","pages":"1052-1055"},"PeriodicalIF":0.0000,"publicationDate":"2017-06-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S2056989017008568","citationCount":"7","resultStr":"{\"title\":\"Crystal structure of 4-[(3-methyl-but-3-eno-yl)-oxy]phenyl 4-<i>n</i>-hexyl-oxybenzoate.\",\"authors\":\"Lyudmila G Kuz'mina, Ivan I Konstantinov, Andrei V Churakov, Mger A Navasardyan\",\"doi\":\"10.1107/S2056989017008568\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>The structure of the title compound, C<sub>23</sub>H<sub>26</sub>O<sub>5</sub> or CH<sub>2</sub>=C(CH<sub>3</sub>)-C(O)O-C<sub>6</sub>H<sub>4</sub>-O(O)C-C<sub>6</sub>H<sub>4</sub>-OC<sub>6</sub>H<sub>13</sub>, has been determined. The mol-ecule is non-planar and the dihedral angle between the phenyl rings is 50.72 (4)°. The crystal packing differs from those typical for mesogenic compounds. Only a weak directional inter-action of the C-H⋯O type combines mol-ecules in endless chains running along the <i>a</i> axis.</p>\",\"PeriodicalId\":7015,\"journal\":{\"name\":\"Acta Crystallographica Section E Crystallographic Communications\",\"volume\":\" \",\"pages\":\"1052-1055\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2017-06-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1107/S2056989017008568\",\"citationCount\":\"7\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Acta Crystallographica Section E Crystallographic Communications\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1107/S2056989017008568\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"2017/7/1 0:00:00\",\"PubModel\":\"eCollection\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Crystallographica Section E Crystallographic Communications","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1107/S2056989017008568","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2017/7/1 0:00:00","PubModel":"eCollection","JCR":"","JCRName":"","Score":null,"Total":0}
Crystal structure of 4-[(3-methyl-but-3-eno-yl)-oxy]phenyl 4-n-hexyl-oxybenzoate.
The structure of the title compound, C23H26O5 or CH2=C(CH3)-C(O)O-C6H4-O(O)C-C6H4-OC6H13, has been determined. The mol-ecule is non-planar and the dihedral angle between the phenyl rings is 50.72 (4)°. The crystal packing differs from those typical for mesogenic compounds. Only a weak directional inter-action of the C-H⋯O type combines mol-ecules in endless chains running along the a axis.