布拉格定律在电子衍射和显微术中的意义,以及布拉格第二定律。

IF 1.8 4区 材料科学
Acta Crystallographica Section A Pub Date : 2013-01-01 Epub Date: 2012-12-05 DOI:10.1107/S0108767312047587
C J Humphreys
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引用次数: 28

摘要

布拉格第二定律,值得更广泛的了解,叙述。然后讨论了布拉格定律在电子衍射和显微镜中的意义,特别强调了x射线和电子衍射的区别。作为这种差异的一个例子,描述了电子衍射中的临界电压效应。然后证明了在高分辨率电子显微镜下晶体的晶格成像直接揭示了用于成像过程的布拉格平面,与布拉格在他的实空间定律中所描述的完全一致。最后,它展示了如何在2012年,在布拉格定律的一百周年纪念上,第一次在电子显微镜下使用样品发射的x射线识别出单个原子。因此,可以形成晶体在实际空间中的原子分辨率x射线图,给出晶体中不同原子或晶体中单个杂质原子的位置和身份。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The significance of Bragg's law in electron diffraction and microscopy, and Bragg's second law.

Bragg's second law, which deserves to be more widely known, is recounted. The significance of Bragg's law in electron diffraction and microscopy is then discussed, with particular emphasis on differences between X-ray and electron diffraction. As an example of such differences, the critical voltage effect in electron diffraction is described. It is then shown that the lattice imaging of crystals in high-resolution electron microscopy directly reveals the Bragg planes used for the imaging process, exactly as visualized by Bragg in his real-space law. Finally, it is shown how in 2012, for the first time, on the centennial anniversary of Bragg's law, single atoms have been identified in an electron microscope using X-rays emitted from the specimen. Hence atomic resolution X-ray maps of a crystal in real space can be formed which give the positions and identities of the different atoms in the crystal, or of a single impurity atom in the crystal.

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来源期刊
自引率
11.10%
发文量
0
审稿时长
3 months
期刊介绍: Acta Crystallographica Section A: Foundations and Advances publishes articles reporting advances in the theory and practice of all areas of crystallography in the broadest sense. As well as traditional crystallography, this includes nanocrystals, metacrystals, amorphous materials, quasicrystals, synchrotron and XFEL studies, coherent scattering, diffraction imaging, time-resolved studies and the structure of strain and defects in materials. The journal has two parts, a rapid-publication Advances section and the traditional Foundations section. Articles for the Advances section are of particularly high value and impact. They receive expedited treatment and may be highlighted by an accompanying scientific commentary article and a press release. Further details are given in the November 2013 Editorial. The central themes of the journal are, on the one hand, experimental and theoretical studies of the properties and arrangements of atoms, ions and molecules in condensed matter, periodic, quasiperiodic or amorphous, ideal or real, and, on the other, the theoretical and experimental aspects of the various methods to determine these properties and arrangements.
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