{"title":"用于高压实验的高分辨率核磁共振探针","authors":"L. Ballard, C. Reiner, J. Jonas","doi":"10.1006/jmra.1996.0216","DOIUrl":null,"url":null,"abstract":"<div><p>A 300 MHz high-resolution, high-pressure NMR probe which operates in the pressure range of 1 bar to 9 kbar at temperatures of −30 to 100°C is described. Specialized novel design features of the probe are discussed and test spectra showing resolution better than 1 Hz (<3.0 × 10<sup>−9</sup>) for 8 mm samples are presented. Potential biochemical applications of this probe are illustrated by experiments dealing with the pressure-induced unfolding of hen egg white lysozyme.</p></div>","PeriodicalId":16165,"journal":{"name":"Journal of Magnetic Resonance, Series A","volume":"123 1","pages":"Pages 81-86"},"PeriodicalIF":0.0000,"publicationDate":"1996-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmra.1996.0216","citationCount":"27","resultStr":"{\"title\":\"High-Resolution NMR Probe for Experiments at High Pressures\",\"authors\":\"L. Ballard, C. Reiner, J. Jonas\",\"doi\":\"10.1006/jmra.1996.0216\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>A 300 MHz high-resolution, high-pressure NMR probe which operates in the pressure range of 1 bar to 9 kbar at temperatures of −30 to 100°C is described. Specialized novel design features of the probe are discussed and test spectra showing resolution better than 1 Hz (<3.0 × 10<sup>−9</sup>) for 8 mm samples are presented. Potential biochemical applications of this probe are illustrated by experiments dealing with the pressure-induced unfolding of hen egg white lysozyme.</p></div>\",\"PeriodicalId\":16165,\"journal\":{\"name\":\"Journal of Magnetic Resonance, Series A\",\"volume\":\"123 1\",\"pages\":\"Pages 81-86\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1996-11-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1006/jmra.1996.0216\",\"citationCount\":\"27\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Magnetic Resonance, Series A\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1064185896902168\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Magnetic Resonance, Series A","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1064185896902168","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
High-Resolution NMR Probe for Experiments at High Pressures
A 300 MHz high-resolution, high-pressure NMR probe which operates in the pressure range of 1 bar to 9 kbar at temperatures of −30 to 100°C is described. Specialized novel design features of the probe are discussed and test spectra showing resolution better than 1 Hz (<3.0 × 10−9) for 8 mm samples are presented. Potential biochemical applications of this probe are illustrated by experiments dealing with the pressure-induced unfolding of hen egg white lysozyme.
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