{"title":"蜂蜜中氟戊酸残留量的超临界萃取。高效液相色谱法测定。","authors":"J Atienza, J J Jiménez, J L Bernal, M T Martín","doi":"10.1016/0021-9673(93)87016-f","DOIUrl":null,"url":null,"abstract":"<p><p>A method for the analysis of fluvalinate residues in honey from beehives treated with this product to prevent varroatosis is described. The method involves supercritical fluid extraction with carbon dioxide and further analysis by high-performance liquid chromatography on a C18 reversed-phase column, acetonitrile-water (80:20) as mobile phase and detection at 254 nm. This method is simpler than the one in which extraction with organic solvents, thin-layer chromatography and gas chromatography is used.</p>","PeriodicalId":15508,"journal":{"name":"Journal of chromatography","volume":"655 1","pages":"95-9"},"PeriodicalIF":0.0000,"publicationDate":"1993-11-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0021-9673(93)87016-f","citationCount":"28","resultStr":"{\"title\":\"Supercritical fluid extraction of fluvalinate residues in honey. Determination by high-performance liquid chromatography.\",\"authors\":\"J Atienza, J J Jiménez, J L Bernal, M T Martín\",\"doi\":\"10.1016/0021-9673(93)87016-f\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>A method for the analysis of fluvalinate residues in honey from beehives treated with this product to prevent varroatosis is described. The method involves supercritical fluid extraction with carbon dioxide and further analysis by high-performance liquid chromatography on a C18 reversed-phase column, acetonitrile-water (80:20) as mobile phase and detection at 254 nm. This method is simpler than the one in which extraction with organic solvents, thin-layer chromatography and gas chromatography is used.</p>\",\"PeriodicalId\":15508,\"journal\":{\"name\":\"Journal of chromatography\",\"volume\":\"655 1\",\"pages\":\"95-9\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1993-11-26\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1016/0021-9673(93)87016-f\",\"citationCount\":\"28\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of chromatography\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1016/0021-9673(93)87016-f\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of chromatography","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1016/0021-9673(93)87016-f","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Supercritical fluid extraction of fluvalinate residues in honey. Determination by high-performance liquid chromatography.
A method for the analysis of fluvalinate residues in honey from beehives treated with this product to prevent varroatosis is described. The method involves supercritical fluid extraction with carbon dioxide and further analysis by high-performance liquid chromatography on a C18 reversed-phase column, acetonitrile-water (80:20) as mobile phase and detection at 254 nm. This method is simpler than the one in which extraction with organic solvents, thin-layer chromatography and gas chromatography is used.
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