精神药物鉴定研究。9精神药物新物质n -乙基亚甲二氧苯丙胺、n -羟基亚甲二氧苯丙胺、甲氯喹酮、4-甲基氨基苯胺、苯地美trazine、苯美trazine参考标准的制备及各项分析数据

M Shimamine, K Takahashi, Y Nakahara
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引用次数: 0

摘要

研究了n -乙基亚甲基二氧基安非他明、n -羟基亚甲基二氧基安非他明、甲氯喹酮、4-甲基氨基安非他明的参比标准。Phendimetrazine和Phenmetrazine是由商业化学品化学合成的。HPLC法测定其纯度均大于99.8%。测定了标准品的薄层色谱、紫外光谱、红外光谱、高效液相色谱、质谱联用、核磁共振等光谱和色谱图。为了法医鉴定这6种药物,对它们的质量破碎和核磁共振谱进行了讨论。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
[Studies on the identification of psychotropic substances. IX. Preparation and various analytical data of reference standard of new psychotropic substances, N-ethyl methylenedioxyamphetamine, N-hydroxy methylenedioxyamphetamine, mecloqualone, 4-methylaminorex, phendimetrazine and phenmetrazine].

The reference standards of N-Ethyl methylenedioxyamphetamine, N-Hydroxy methylenedioxy-amphetamine, Mecloqualone, 4-Methylaminorex. Phendimetrazine and Phenmetrazine were chemically prepared from commercial chemicals. Their purities determined by HPLC were more than 99.8%. The standard spectra and chromatograms of the standards such as TLC, UV, IR, HPLC, GC/MS and NMR were measured. For the identification of these six drugs in forensic laboratory, their mass fragmentation and NMR spectra were discussed.

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