5-{(E)-[（1h -吲哚-3-酰基甲酰胺）-亚氨基]-甲基}-2-甲基氧基苯基丙烷-1-磺酸盐的合成与晶体结构

IF 0.5 Q4 CRYSTALLOGRAPHY

Acta Crystallographica Section E: Crystallographic Communications Pub Date : 2025-04-01 DOI:10.1107/S2056989025002087

Reham A. Mohamed-Ezzat , Benson M. Kariuki , Aisha A. K. Al-Ashmawy , Aladdin M. Srour

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引用次数: 0

摘要

晶体结构以三维氢键网络为特征。通过N-H⋯O接触形成的链由额外的分子间键连接以完成结构。在标题分子C20H21N3O5S中，甲基-同甲乙肼和甲基-氧苯基几乎共面，吲哚基离平面旋转得更远。晶体结构中的分子通过N-H⋯O氢键相互作用形成平行于a轴方向的链。邻近的链通过N-H⋯O接触连接，形成三维网络。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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Synthesis and crystal structure of 5-{(E)-[(1H-indol-3-ylformamido)imino]methyl}-2-methoxyphenyl propane-1-sulfonate

The crystal structure is characterized by a three-dimensional hydrogen-bonding network. Chains formed through N—H⋯O contacts are linked by additional intermolecular bonds to complete the structure.

In the title molecule, C₂₀H₂₁N₃O₅S, the methylideneformohydrazide and methoxybenzene groups are almost coplanar, with the indolyl group being rotated farther from the plane. The molecules in the crystal structure form chains parallel to the a-axis direction through N—H⋯O hydrogen-bonding interactions. Neighbouring chains are linked by N—H⋯O contacts to form a three-dimensional network.

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来源期刊

Acta Crystallographica Section E: Crystallographic Communications Chemistry-Chemistry (all)

CiteScore

1.90

自引率

0.00%

发文量

351

审稿时长

3 weeks

期刊介绍： Acta Crystallographica Section E: Crystallographic Communications is the IUCr''s open-access structural communications journal. It provides a fast, simple and easily accessible publication mechanism for crystal structure determinations of inorganic, metal-organic and organic compounds. The electronic submission, validation, refereeing and publication facilities of the journal ensure rapid and high-quality publication of fully validated structures. The primary article category is Research Communications; these are peer-reviewed articles describing one or more structure determinations with appropriate discussion of the science.