Xueping Tao, Dan Wang, Meiting Yan, Yan Ma, Yang Zhou, Qifeng Fu
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Recent Advances in the Construction and Applications of Monolithic and Open-tubular Capillary Electrochromatography (2022–2024)
Capillary electrochromatography (CEC) has attracted significant attention and gained considerable recognition in the field of separation science owing to its excellent separation efficiency. While numerous reviews on CEC have been published in recent years, a comprehensive and systematic summary of the typical synthesis strategies for electrochromatographic stationary phases and their state-of-the-art applications in CEC remains lacking. This review highlights recent advances (over the past 3 years) and representative applications (including chiral separation, microextraction-coupled analysis, metabolomics, enzyme analysis, and food analysis) of monolithic and open-tubular stationary phases in CEC. The advantages and limitations of each methodology are critically analyzed to present a balanced evaluation. Additionally, this work outlines future prospects regarding the development trends in electrochromatographic stationary phase preparation methods and the evolving applications of CEC.
期刊介绍：
The Journal of Separation Science (JSS) is the most comprehensive source in separation science, since it covers all areas of chromatographic and electrophoretic separation methods in theory and practice, both in the analytical and in the preparative mode, solid phase extraction, sample preparation, and related techniques. Manuscripts on methodological or instrumental developments, including detection aspects, in particular mass spectrometry, as well as on innovative applications will also be published. Manuscripts on hyphenation, automation, and miniaturization are particularly welcome. Pre- and post-separation facets of a total analysis may be covered as well as the underlying logic of the development or application of a method.
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