表面活性剂OP-10的增强对甲基三甲氧基硅烷耐蚀性能的优化

IF 0.9 4区 化学 Q4 CHEMISTRY, MULTIDISCIPLINARY
Z. Zhou, L. Qiu, G. Hu, Z. Pan, G. Sun, Z. Sun
{"title":"表面活性剂OP-10的增强对甲基三甲氧基硅烷耐蚀性能的优化","authors":"Z. Zhou,&nbsp;L. Qiu,&nbsp;G. Hu,&nbsp;Z. Pan,&nbsp;G. Sun,&nbsp;Z. Sun","doi":"10.1134/S1070363224612663","DOIUrl":null,"url":null,"abstract":"<p>Using an immersion method, an organic methyltrimethoxysilane (MTMS) coating was prepared on the surface of aluminum alloys at room temperature. A more corrosion-resistant coating has been successfully developed by optimizing hydrolysis conditions, adding surfactant OP-10 and conducting maturation treatment. To characterize the solution, a conductivity meter, transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), and a particle size analyzer were utilized. As for the analysis of the surface properties of the samples, a series of methods such as X-ray photoelectron spectroscopy (XPS), attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), contact angle measurements, scanning electron microscopy (SEM), electrochemical impedance spectroscopy (EIS), and Tafel polarization analysis were adopted. The results showed that the synergistic effect of OP-10 and maturation treatment can significantly improve the corrosion resistance of the coating.</p>","PeriodicalId":761,"journal":{"name":"Russian Journal of General Chemistry","volume":"95 1","pages":"253 - 265"},"PeriodicalIF":0.9000,"publicationDate":"2025-02-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Optimizing the Corrosion Resistance of Methyltrimethoxysilane with the Enhancement of Surfactant OP-10\",\"authors\":\"Z. Zhou,&nbsp;L. Qiu,&nbsp;G. Hu,&nbsp;Z. Pan,&nbsp;G. Sun,&nbsp;Z. Sun\",\"doi\":\"10.1134/S1070363224612663\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Using an immersion method, an organic methyltrimethoxysilane (MTMS) coating was prepared on the surface of aluminum alloys at room temperature. A more corrosion-resistant coating has been successfully developed by optimizing hydrolysis conditions, adding surfactant OP-10 and conducting maturation treatment. To characterize the solution, a conductivity meter, transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), and a particle size analyzer were utilized. As for the analysis of the surface properties of the samples, a series of methods such as X-ray photoelectron spectroscopy (XPS), attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), contact angle measurements, scanning electron microscopy (SEM), electrochemical impedance spectroscopy (EIS), and Tafel polarization analysis were adopted. The results showed that the synergistic effect of OP-10 and maturation treatment can significantly improve the corrosion resistance of the coating.</p>\",\"PeriodicalId\":761,\"journal\":{\"name\":\"Russian Journal of General Chemistry\",\"volume\":\"95 1\",\"pages\":\"253 - 265\"},\"PeriodicalIF\":0.9000,\"publicationDate\":\"2025-02-27\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Russian Journal of General Chemistry\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1070363224612663\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of General Chemistry","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S1070363224612663","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0

摘要

采用浸泡法制备了室温下铝合金表面的有机甲基三甲氧基硅烷(MTMS)涂层。通过优化水解条件、添加表面活性剂OP-10并进行成熟处理,成功开发出一种耐腐蚀涂层。利用电导率仪、透射电子显微镜(TEM)、傅里叶变换红外光谱(FTIR)和粒度分析仪对溶液进行表征。采用x射线光电子能谱(XPS)、衰减全反射傅立叶变换红外光谱(ATR-FTIR)、接触角测量、扫描电镜(SEM)、电化学阻抗谱(EIS)、Tafel极化分析等一系列方法分析样品的表面性质。结果表明,OP-10与成熟处理的协同作用可显著提高涂层的耐蚀性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Optimizing the Corrosion Resistance of Methyltrimethoxysilane with the Enhancement of Surfactant OP-10

Optimizing the Corrosion Resistance of Methyltrimethoxysilane with the Enhancement of Surfactant OP-10

Using an immersion method, an organic methyltrimethoxysilane (MTMS) coating was prepared on the surface of aluminum alloys at room temperature. A more corrosion-resistant coating has been successfully developed by optimizing hydrolysis conditions, adding surfactant OP-10 and conducting maturation treatment. To characterize the solution, a conductivity meter, transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), and a particle size analyzer were utilized. As for the analysis of the surface properties of the samples, a series of methods such as X-ray photoelectron spectroscopy (XPS), attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), contact angle measurements, scanning electron microscopy (SEM), electrochemical impedance spectroscopy (EIS), and Tafel polarization analysis were adopted. The results showed that the synergistic effect of OP-10 and maturation treatment can significantly improve the corrosion resistance of the coating.

求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
CiteScore
1.40
自引率
22.20%
发文量
252
审稿时长
2-4 weeks
期刊介绍: Russian Journal of General Chemistry is a journal that covers many problems that are of general interest to the whole community of chemists. The journal is the successor to Russia’s first chemical journal, Zhurnal Russkogo Khimicheskogo Obshchestva (Journal of the Russian Chemical Society ) founded in 1869 to cover all aspects of chemistry. Now the journal is focused on the interdisciplinary areas of chemistry (organometallics, organometalloids, organoinorganic complexes, mechanochemistry, nanochemistry, etc.), new achievements and long-term results in the field. The journal publishes reviews, current scientific papers, letters to the editor, and discussion papers.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信