高效液相色谱串联质谱法测定饲料和饲料添加剂中的脂溶性维生素

IF 0.8 4区物理与天体物理 Q4 OPTICS

Optics and Spectroscopy Pub Date : 2024-09-16 DOI:10.1134/S0030400X24700395

A. Z. Ispiryan, J. S. Mysina, I. V. Batov, S. V. Belov, I. S. Nesterenko

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引用次数: 0

摘要

本文介绍了一种高效液相色谱-质谱法测定饲料、饲料添加剂中脂溶性维生素的方法。维生素质量浓度的测量范围：a为0.35-14.0 mg/kg， d3为0.0065-1.0 mg/kg， e为0.63-50.0 mg/kg。该技术是基于样品的碱性水解和正己烷提取脂溶性维生素。所得提取物采用高效液相色谱-质谱检测（HPLC MS/MS）进行分析。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

Determination of Fat-Soluble Vitamins by High-Performance Liquid Chromatography Tandem Mass Spectrometry in Feed, Feed Additives

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Determination of Fat-Soluble Vitamins by High-Performance Liquid Chromatography Tandem Mass Spectrometry in Feed, Feed Additives

This article describes the development of a technique for the determination of fat-soluble vitamins using high-performance liquid chromatography with mass spectrometric detection in feed, feed additives. Measurement ranges of mass concentrations of vitamins: A—from 0.35–14.0 mg/kg, D₃—from 0.0065–1.0 mg/kg, and E—from 0.63–50.0 mg/kg. The technique is based on alkaline hydrolysis of the sample and extraction of fat-soluble vitamins with hexane. The analysis of the obtained extracts is carried out by high-performance liquid chromatography with mass spectrometric detection (HPLC MS/MS).

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来源期刊

Optics and Spectroscopy 物理-光谱学

CiteScore

1.60

自引率

0.00%

发文量

审稿时长

4.5 months

期刊介绍： Optics and Spectroscopy (Optika i spektroskopiya), founded in 1956, presents original and review papers in various fields of modern optics and spectroscopy in the entire wavelength range from radio waves to X-rays. Topics covered include problems of theoretical and experimental spectroscopy of atoms, molecules, and condensed state, lasers and the interaction of laser radiation with matter, physical and geometrical optics, holography, and physical principles of optical instrument making.