建立同时测定含芦荟提取物的化妆品中尿囊素和 D-泛醇的 HPLC-UV 方法

IF 1.7 4区化学 Q3 CHEMISTRY, ANALYTICAL

Acta Chromatographica Pub Date : 2024-05-21 DOI:10.1556/1326.2024.01216

Burhan Ceylan, Ş. E. KEPEKÇİ TEKKELİ

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引用次数: 0

摘要

本研究建立了一种简单、快速、选择性强的分析方法，用于同时测定含芦荟提取物的化妆品中尿囊素和D-泛醇的含量。该方法采用反相液相色谱法，流动相为乙腈-10 mM 磷酸（pH 2.5）（85:15, v/v），柱温为 30 ℃的 C18 色谱柱。采用紫外-可见检测器检测分析物，检测波长为 210 nm。进样量为 20 μL。尿囊素和 D-泛醇的线性范围分别为 0.2-20 和 0.1-10 μg mL-1。尿囊素和 D-泛醇的检出限（LOD）分别为 0.07 μg mL-1 和 0.03 μg mL-1，定量限（LOQ）分别为 0.2 μg mL-1 和 0.1 μg mL-1。未发现伴随物的干扰。所开发的方法被用于分析 10 种不同类型的化妆品。预计该方法可用于对含有尿囊素和 D-泛醇的化妆品进行常规分析、质量控制和标准化。

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Development of an HPLC-UV method for the simultaneous determination of allantoin and D-panthenol in cosmetic products containing Aloe vera extracts

A simple, fast and selective analytical method has been developed for the simultaneous determination of allantoin and D-panthenol in cosmetic products containing Aloe vera extracts. The proposed method depends on reversed-phase liquid chromatography with isocratic flow profile of the mobile phase composed of acetonitrile–10 mM phosphoric acid (pH 2.5) (85:15, v/v), with a C18 column at 30 °C. The analytes were detected with UV–vis. detector at 210 nm. The injection volume was 20 μL. The linearity ranges were found to be 0.2–20 and 0.1–10 μg mL−1 for allantoin and D-panthenol, respectively. LOD values were found to be 0.07 μg mL−1 and 0.03 μg mL−1, LOQ values were found to be 0.2 and 0.1 μg mL−1 for allantoin and D-panthenol, respectively. No interference was observed from concomitants. The developed method was applied to the analysis of 10 different type cosmetic products. It is foreseen that the method will be able to be used in order to carry out routine analysis, quality control and standardization in cosmetic products containing allantoin and D-panthenol.

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来源期刊

Acta Chromatographica 化学-分析化学

CiteScore

4.00

自引率

0.00%

发文量

审稿时长

2.3 months

期刊介绍： Acta Chromatographica Open Access Acta Chromatographica publishes peer-reviewed scientific articles on every field of chromatography, including theory of chromatography; progress in synthesis and characterization of new stationary phases; chromatography of organic, inorganic and complex compounds; enantioseparation and chromatography of chiral compounds; applications of chromatography in biology, pharmacy, medicine, and food analysis; environmental applications of chromatography; analytical and physico-chemical aspects of sample preparation for chromatography; hyphenated and combined techniques; chemometrics and its applications in separation science.