硅烷偶联剂的不同水量和水解时间对二硅酸锂玻璃陶瓷和复合树脂剪切粘接强度的影响

IF 16.4 1区化学 Q1 CHEMISTRY, MULTIDISCIPLINARY

Accounts of Chemical Research Pub Date : 2024-04-05 DOI:10.4012/dmj.2023-190

Pimchanok Osotprasit, Sasipin Lauvahutanon, Yosnarong Sirimethawong, Patcharanun Chaiamornsup, P. Jiangkongkho

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引用次数: 0

摘要

本研究旨在评估不同水量和水解时间的硅烷偶联剂对二硅酸锂玻璃陶瓷（LDS）与复合树脂之间剪切粘接强度的影响。制备了 14 组（n=7）不同水量（90、50 和 10%v/v ）和水解时间（5、19、75 和 300 秒）的实验硅烷偶联剂，分别用于硅烷化组、非硅烷化组和商用硅烷偶联剂（CSC）组。双向方差分析（ANOVA）显示，ESC 的水量和水解时间对 LDS 和复合树脂之间的剪切粘接强度没有交互作用。单因素方差分析显示，50%v/v 组的剪切粘接强度最高，混合失效模式的平均百分比最高。13C 和 29Si 分子分析表明，在 50%v/v 组中发现了 M2 和 M3 水解物种的核磁共振谱。M2 和 M3 的出现是导致剪切粘接强度最高的主要因素。

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Effect of the difference water amounts and hydrolysis times of silane coupling agent on the shear bond strength between lithium disilicate glass ceramic and composite resin.

This study was to evaluate the effect of different water amounts and hydrolysis times of silane coupling agent on shear bond strength between lithium disilicate glass ceramic (LDS) and composite resin. Fourteen groups (n=7) of different water amounts (90, 50 and 10%v/v) and hydrolysis times (5, 19, 75 and 300 s) of experimental silane coupling agent that were prepared for silanization, non-silanization and commercial silane coupling agent (CSC) groups. Two-way analysis of variance (ANOVA) revealed no interaction between water amounts and hydrolysis times of ESC on shear bond strength between LDS and composite resin. One-way ANOVA exhibited the highest shear bond strength and the highest mean percentage in mixed failure mode in the 50%v/v group. Molecular analysis of 13C and 29Si indicated that nuclear magnetic resonance spectra of M2 and M3 hydrolysis species were found in 50%v/v group. The presenting of M2 and M3 which was predominant factor contributing to the highest shear bond strength.

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来源期刊

Accounts of Chemical Research 化学-化学综合

CiteScore

31.40

自引率

1.10%

发文量

312

审稿时长

2 months

期刊介绍： Accounts of Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry and biochemistry. These short reviews focus on research from the author’s own laboratory and are designed to teach the reader about a research project. In addition, Accounts of Chemical Research publishes commentaries that give an informed opinion on a current research problem. Special Issues online are devoted to a single topic of unusual activity and significance. Accounts of Chemical Research replaces the traditional article abstract with an article "Conspectus." These entries synopsize the research affording the reader a closer look at the content and significance of an article. Through this provision of a more detailed description of the article contents, the Conspectus enhances the article's discoverability by search engines and the exposure for the research.