超碱氧化钙催化剂在酰胺化法合成硬脂酰胺表面活性剂中的应用

Q4 Engineering

ARPN Journal of Engineering and Applied Sciences Pub Date : 2024-01-30 DOI:10.59018/1123301

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引用次数: 0

摘要

表面活性剂是一种可以降低表面张力的物质，它在一个分子中有两个基团：亲水基团和疏水基团。在同一分子中，这两个基团具有不同的极性。在这项研究中，使用超碱氧化钙催化剂，在正己烷和异丙醇混合溶剂中将硬脂酸与尿素酰胺化。研究通过观察两个与工艺无关的变量来进行：反应温度范围为 55˚C、65˚C 和 75˚C，反应时间范围为 2 小时、3 小时和 4 小时。在温度为 75˚C 和反应时间为 3 小时的条件下，获得了最佳条件，转化率为 89.88%。然后使用傅立叶变换红外光谱和超碱式氧化钙催化剂对研究样品进行了分析，并使用扫描电子显微镜对其形态特性进行了分析。

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Application of super base calcium oxide catalyst in the synthesis of stearamide surfactants by amidation

Surfactant is a substance that can reduce surface tension, which has two groups in one molecule: hydrophilic and hydrophobic. These two groups, in the same molecule, have different degrees of polarity. In this study, stearic acid was amidated with urea using a super base calcium oxide catalyst in a mixture of hexane and isopropanol solvents. The study was carried out by observing two process-independent variables: the reaction temperature in the range of 55˚C, 65˚C, and 75˚C, and the reaction time in the range of 2 hours, 3 hours, and 4 hours. Optimum conditions were obtained at a temperature of 75°C and a reaction time of 3 hours, where a conversion of 89.88% was obtained. Then the research samples were analyzed using FT-IR and super base calcium oxide catalyst and analyzed for morphological properties using SEM.

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来源期刊

ARPN Journal of Engineering and Applied Sciences Engineering-Engineering (all)

CiteScore

0.70

自引率

0.00%

发文量

期刊介绍： ARPN Journal of Engineering and Applied Sciences (ISSN 1819-6608) is an online peer-reviewed International research journal aiming at promoting and publishing original high quality research in all disciplines of engineering sciences and technology. All research articles submitted to ARPN-JEAS should be original in nature, never previously published in any journal or presented in a conference or undergoing such process across the globe. All the submissions will be peer-reviewed by the panel of experts associated with particular field. Submitted papers should meet the internationally accepted criteria and manuscripts should follow the style of the journal for the purpose of both reviewing and editing. Our mission is -In cooperation with our business partners, lower the world-wide cost of research publishing operations. -Provide an infrastructure that enriches the capacity for research facilitation and communication, among researchers, college and university teachers, students and other related stakeholders. -Reshape the means for dissemination and management of information and knowledge in ways that enhance opportunities for research and learning and improve access to scholarly resources. -Expand access to research publishing to the public. -Ensure high-quality, effective and efficient production and support good research and development activities that meet or exceed the expectations of research community. Scope of Journal of Engineering and Applied Sciences: -Engineering Mechanics -Construction Materials -Surveying -Fluid Mechanics & Hydraulics -Modeling & Simulations -Thermodynamics -Manufacturing Technologies -Refrigeration & Air-conditioning -Metallurgy -Automatic Control Systems -Electronic Communication Systems -Agricultural Machinery & Equipment -Mining & Minerals -Mechatronics -Applied Sciences -Public Health Engineering -Chemical Engineering -Hydrology -Tube Wells & Pumps -Structures