带有 Ugi 4CR 修饰侧链的胆汁酸衍生物的合成与 NMR 表征

IF 1.1 4区化学 Q3 CHEMISTRY, MULTIDISCIPLINARY

Journal of the Mexican Chemical Society Pub Date : 2024-02-09 DOI:10.29356/jmcs.v68i2.2061

Josué Vazquez-Chavez, Brian A. Verdeja-Perdomo, M. A. Iglesias‐Arteaga

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引用次数: 0

摘要

摘要介绍了应用四组份 Ugi 反应合成五种具有修饰侧链的胆汁酸衍生物的过程，并给出了明确的结构特征、功能 1H NMR 信号的分配以及所有 13C{1H} NMR 化学位移。摘要介绍了应用四组分 Ugi 反应合成带有修饰侧链的五种胆汁酸衍生物的过程。介绍了 1H NMR 功能信号和所有 13C{1H} NMR 化学位移的明确结构特征和分配。

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Synthesis and NMR characterization of Bile Acid Derivatives Bearing Ugi 4CR-Modified Side Chains

Abstract. The application of the four-component Ugi reaction for the synthesis of five bile acid derivatives bearing modified side chains is described. The unambiguous structural characterization and assignment of the functional 1H NMR signals and all 13C{1H} NMR chemical shifts are presented. Resumen. Se describe la aplicación de la reacción de cuatro componentes de Ugi a la síntesis de cinco derivados de ácidos biliares que portan cadenas laterales modificadas. Se presenta la caracterización estructural inequívoca y la asignación de las señales funcionales de 1H RMN y de todos los desplazamientos químicos de 13C{1H} RMN.

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来源期刊

Journal of the Mexican Chemical Society 化学-化学综合

CiteScore

2.00

自引率

0.00%

发文量

审稿时长

6-12 weeks

期刊介绍： The Journal of the Mexican Chemical Society (J. Mex. Chem. Soc.) is a scientific, blind, peer reviewed, and open access, free of charge publication that covers all areas of chemistry and its sub-disciplines (i.e. medicinal chemistry, natural products, electrochemistry, material science, computational chemistry, organic chemistry, bionirganic chemistry, etc). It is devoted to facilitating the worldwide advancement of our understanding of chemistry. It will primarily publish original contributions of research in all branches of the theory and practice of chemistry in its broadest context as well as critical reviews in active areas of chemical research where the author has published significant contribution. The J. Mex. Chem. Soc. is a quarterly publication which language of submission and publication is English. To be suitable for publication in J. Mex. Chem. Soc., manuscripts must describe novel aspects of chemistry, high quality of results and discussion an excellent bibliographic support, and contribute to the development of the field. Routine or incremental work are not suitable for publication in J. Mex. Chem. Soc. Authors are encouraged to send contributions in electronic form. Our online submission system guides you stepwise through the process of entering your article details and uploading your files.