Bakr F. Abdel-Wahab, H. Mohamed, Benson M. Kariuki, Gamal A. El-Hiti
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引用次数: 0
摘要
将(E)-2-(4-氟亚苄基)-3,4-二氢萘-1(2H)-酮和(2,4-二硝基苯基)肼在含有盐酸（0.2 mL；37%）的沸腾乙醇中反应 1.5 小时，得到 1-(2,4-二硝基苯基)-2-(2-(4-氟亚苄基)-3,4-二氢萘-1(2H)-亚基)肼，产率为 90%。通过核磁共振等各种光谱分析和 X 射线晶体学分析，确定了新合成的腙的结构。
The reaction of (E)-2-(4-fluorobenzylidene)-3,4-dihydronaphthalen-1(2H)-one and (2,4-dinitrophenyl)hydrazine in boiling ethanol containing hydrochloric acid (0.2 mL; 37%) for 1.5 h gave 1-(2,4-dinitrophenyl)-2-(2-(4-fluorobenzylidene)-3,4-dihydronaphthalen-1(2H)-ylidene)hydrazine in a 90% yield. Various spectral analyses, including NMR, and X-ray crystallography established the structure of the newly synthesized hydrazone.
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