O. L. Belousova, A. N. Parunova, N. Yu. Fedorenko, V. L. Ugolkov, T. V. Khamova, O. A. Shilova
{"title":"Xerogel 和粉末合成条件对 ZrO_2-СeO_2-Al_2O_3 体系中基于 t-ZrO_2 的陶瓷特性的影响","authors":"O. L. Belousova, A. N. Parunova, N. Yu. Fedorenko, V. L. Ugolkov, T. V. Khamova, O. A. Shilova","doi":"10.1134/S1087659623600667","DOIUrl":null,"url":null,"abstract":"<p>Xerogels and powders of a solid solution based on zirconium dioxide are synthesized by the method of coprecipitation of hydroxides from aqueous solutions of salts of zirconium nitrate ZrO(NO<sub>3</sub>)<sub>2</sub>⋅2H<sub>2</sub>O, aluminum Al(NO<sub>3</sub>)<sub>3</sub>⋅9H<sub>2</sub>O, and cerium Ce(NO<sub>3</sub>)<sub>3</sub>⋅9H<sub>2</sub>O with an aqueous 1 M solution of ammonia NH<sub>4</sub>OH. A dense ceramic with low porosity and water absorption is obtained. The effect of the ultrasonic treatment of the precipitate and mechanical treatment of the xerogel on the physicochemical properties of the obtained materials is evaluated.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 6","pages":"664 - 671"},"PeriodicalIF":0.8000,"publicationDate":"2023-12-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of Xerogel and Powder Synthesis Conditions on the Properties of Ceramics Based on t-ZrO2 in the ZrO2–СeO2–Al2O3 System\",\"authors\":\"O. L. Belousova, A. N. Parunova, N. Yu. Fedorenko, V. L. Ugolkov, T. V. Khamova, O. A. Shilova\",\"doi\":\"10.1134/S1087659623600667\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Xerogels and powders of a solid solution based on zirconium dioxide are synthesized by the method of coprecipitation of hydroxides from aqueous solutions of salts of zirconium nitrate ZrO(NO<sub>3</sub>)<sub>2</sub>⋅2H<sub>2</sub>O, aluminum Al(NO<sub>3</sub>)<sub>3</sub>⋅9H<sub>2</sub>O, and cerium Ce(NO<sub>3</sub>)<sub>3</sub>⋅9H<sub>2</sub>O with an aqueous 1 M solution of ammonia NH<sub>4</sub>OH. A dense ceramic with low porosity and water absorption is obtained. The effect of the ultrasonic treatment of the precipitate and mechanical treatment of the xerogel on the physicochemical properties of the obtained materials is evaluated.</p>\",\"PeriodicalId\":580,\"journal\":{\"name\":\"Glass Physics and Chemistry\",\"volume\":\"49 6\",\"pages\":\"664 - 671\"},\"PeriodicalIF\":0.8000,\"publicationDate\":\"2023-12-27\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Glass Physics and Chemistry\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1087659623600667\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Glass Physics and Chemistry","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1134/S1087659623600667","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
Effect of Xerogel and Powder Synthesis Conditions on the Properties of Ceramics Based on t-ZrO2 in the ZrO2–СeO2–Al2O3 System
Xerogels and powders of a solid solution based on zirconium dioxide are synthesized by the method of coprecipitation of hydroxides from aqueous solutions of salts of zirconium nitrate ZrO(NO3)2⋅2H2O, aluminum Al(NO3)3⋅9H2O, and cerium Ce(NO3)3⋅9H2O with an aqueous 1 M solution of ammonia NH4OH. A dense ceramic with low porosity and water absorption is obtained. The effect of the ultrasonic treatment of the precipitate and mechanical treatment of the xerogel on the physicochemical properties of the obtained materials is evaluated.
期刊介绍:
Glass Physics and Chemistry presents results of research on the inorganic and physical chemistry of glass, ceramics, nanoparticles, nanocomposites, and high-temperature oxides and coatings. The journal welcomes manuscripts from all countries in the English or Russian language.