{"title":"烧结温度对Mg0,92Zn0,05C0,03合金晶体结构和物理性能的影响","authors":"Budiarto Budiarto, Susilo Susilo","doi":"10.30811/jpl.v21i3.3719","DOIUrl":null,"url":null,"abstract":"The effect of sintering temperature on the crystal structure and physical properties of the Mg0,92Zn0,05C0,03 alloy has been studied. Magnesium-based alloys are one of the alloys that have been used in industry, the health sector, and as biodegradable materials and biomaterials. The aim of this study was to determine the effect of temperature and sintering holding time on crystal size, dislocation density, microlattice strain, and yield strength, porosity and density of Mg0,92Zn0,05C0,03 alloy. The results of testing the crystal structure of the alloy Mg0,92Zn0,05C0,03 with an X-ray diffractometer showed several diffraction peaks consisting of the main phase α–Mg and a small part of the MgZn phase. Testing of Mg0,92Zn0,05C0,03 alloy after sintering with variations in temperature and 90 minutes holding time for crystal size showed that the higher the sintering temperature (425 0C to 575 0C) the crystal size value decreased significantly from 82.36 nm to 18.75 nm, and the dislocation density increased from 0.113 to 0.868 lines/mm2. For micro strain decreased from 0.015 to 0.0087. However, in the very small porosity test, the increase was from 29.8% to 31.9%. As well as for density (1.8 gr/cm3) and yield strength (274 MPa) there was no significant decrease of around 1.4%, but the synthesized Mg0,92Zn0,05C0,03 alloy fulfilled as a bone implant bio material.hhThe effect of sintering temperature on the crystal structure and physical properties of the Mg0,92Zn0,05C0,03 alloy has been studied. Magnesium-based alloys are one of the alloys that have been used in industry, the health sector, and as biodegradable materials and biomaterials. The aim of this study was to determine the effect of temperature and sintering holding time on crystal size, dislocation density, microlattice strain, and yield strength, porosity and density of Mg0,92Zn0,05C0,03 alloy. The results of testing the crystal structure of the alloy Mg0,92Zn0,05C0,03 with an X-ray diffractometer showed several diffraction peaks consisting of the main phase α–Mg and a small part of the MgZn phase. Testing of Mg0,92Zn0,05C0,03 alloy after sintering with variations in temperature and 90 minutes holding time for crystal size showed that the higher the sintering temperature (425 0C to 575 0C) the crystal size value decreased significantly from 82.36 nm to 18.75 nm, and the dislocation density increased from 0.113 to 0.868 lines/mm2. For micro strain decreased from 0.015 to 0.0087. However, in the very small porosity test, the increase was from 29.8% to 31.9%. As well as for density (1.8 gr/cm3) and yield strength (274 MPa) there was no significant decrease of around 1.4%, but the synthesized Mg0,92Zn0,05C0,03 alloy fulfilled as a bone implant bio material.","PeriodicalId":166128,"journal":{"name":"Jurnal POLIMESIN","volume":"29 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-06-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of sintering temperature on crystal structure and physical properties of the Mg0,92Zn0,05C0,03 Alloy\",\"authors\":\"Budiarto Budiarto, Susilo Susilo\",\"doi\":\"10.30811/jpl.v21i3.3719\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The effect of sintering temperature on the crystal structure and physical properties of the Mg0,92Zn0,05C0,03 alloy has been studied. Magnesium-based alloys are one of the alloys that have been used in industry, the health sector, and as biodegradable materials and biomaterials. The aim of this study was to determine the effect of temperature and sintering holding time on crystal size, dislocation density, microlattice strain, and yield strength, porosity and density of Mg0,92Zn0,05C0,03 alloy. The results of testing the crystal structure of the alloy Mg0,92Zn0,05C0,03 with an X-ray diffractometer showed several diffraction peaks consisting of the main phase α–Mg and a small part of the MgZn phase. Testing of Mg0,92Zn0,05C0,03 alloy after sintering with variations in temperature and 90 minutes holding time for crystal size showed that the higher the sintering temperature (425 0C to 575 0C) the crystal size value decreased significantly from 82.36 nm to 18.75 nm, and the dislocation density increased from 0.113 to 0.868 lines/mm2. For micro strain decreased from 0.015 to 0.0087. However, in the very small porosity test, the increase was from 29.8% to 31.9%. As well as for density (1.8 gr/cm3) and yield strength (274 MPa) there was no significant decrease of around 1.4%, but the synthesized Mg0,92Zn0,05C0,03 alloy fulfilled as a bone implant bio material.hhThe effect of sintering temperature on the crystal structure and physical properties of the Mg0,92Zn0,05C0,03 alloy has been studied. Magnesium-based alloys are one of the alloys that have been used in industry, the health sector, and as biodegradable materials and biomaterials. The aim of this study was to determine the effect of temperature and sintering holding time on crystal size, dislocation density, microlattice strain, and yield strength, porosity and density of Mg0,92Zn0,05C0,03 alloy. The results of testing the crystal structure of the alloy Mg0,92Zn0,05C0,03 with an X-ray diffractometer showed several diffraction peaks consisting of the main phase α–Mg and a small part of the MgZn phase. Testing of Mg0,92Zn0,05C0,03 alloy after sintering with variations in temperature and 90 minutes holding time for crystal size showed that the higher the sintering temperature (425 0C to 575 0C) the crystal size value decreased significantly from 82.36 nm to 18.75 nm, and the dislocation density increased from 0.113 to 0.868 lines/mm2. For micro strain decreased from 0.015 to 0.0087. However, in the very small porosity test, the increase was from 29.8% to 31.9%. As well as for density (1.8 gr/cm3) and yield strength (274 MPa) there was no significant decrease of around 1.4%, but the synthesized Mg0,92Zn0,05C0,03 alloy fulfilled as a bone implant bio material.\",\"PeriodicalId\":166128,\"journal\":{\"name\":\"Jurnal POLIMESIN\",\"volume\":\"29 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-06-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Jurnal POLIMESIN\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.30811/jpl.v21i3.3719\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Jurnal POLIMESIN","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30811/jpl.v21i3.3719","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
研究了烧结温度对Mg0,92Zn0,05C0,03合金晶体结构和物理性能的影响。镁基合金是应用于工业、卫生、生物降解材料和生物材料的合金之一。研究了温度和烧结保温时间对Mg0,92Zn0,05C0,03合金晶粒尺寸、位错密度、微晶格应变、屈服强度、孔隙率和密度的影响。用x射线衍射仪对Mg0,92Zn0,05C0,03合金的晶体结构进行了测试,结果表明,有几个衍射峰主要为α-Mg相和一小部分MgZn相。对Mg0、92Zn0、055c0、03合金烧结后的温度变化和90分钟的晶粒尺寸保温时间进行测试表明,烧结温度越高(425℃~ 575℃),晶粒尺寸值从82.36 nm显著降低到18.75 nm,位错密度从0.113 lines/mm2增加到0.868 lines/mm2。微应变由0.015降至0.0087。而在非常小孔隙度测试中,从29.8%增加到31.9%。在密度(1.8 g /cm3)和屈服强度(274 MPa)方面,合成的Mg0,92Zn0,05C0,03合金没有明显的下降(约1.4%),但可以作为植骨生物材料。研究了烧结温度对Mg0,92Zn0,05C0,03合金晶体结构和物理性能的影响。镁基合金是应用于工业、卫生、生物降解材料和生物材料的合金之一。研究了温度和烧结保温时间对Mg0,92Zn0,05C0,03合金晶粒尺寸、位错密度、微晶格应变、屈服强度、孔隙率和密度的影响。用x射线衍射仪对Mg0,92Zn0,05C0,03合金的晶体结构进行了测试,结果表明,有几个衍射峰主要为α-Mg相和一小部分MgZn相。对Mg0、92Zn0、055c0、03合金烧结后的温度变化和90分钟的晶粒尺寸保温时间进行测试表明,烧结温度越高(425℃~ 575℃),晶粒尺寸值从82.36 nm显著降低到18.75 nm,位错密度从0.113 lines/mm2增加到0.868 lines/mm2。微应变由0.015降至0.0087。而在非常小孔隙度测试中,从29.8%增加到31.9%。在密度(1.8 g /cm3)和屈服强度(274 MPa)方面,合成的Mg0,92Zn0,05C0,03合金没有明显的下降(约1.4%),但可以作为植骨生物材料。
Effect of sintering temperature on crystal structure and physical properties of the Mg0,92Zn0,05C0,03 Alloy
The effect of sintering temperature on the crystal structure and physical properties of the Mg0,92Zn0,05C0,03 alloy has been studied. Magnesium-based alloys are one of the alloys that have been used in industry, the health sector, and as biodegradable materials and biomaterials. The aim of this study was to determine the effect of temperature and sintering holding time on crystal size, dislocation density, microlattice strain, and yield strength, porosity and density of Mg0,92Zn0,05C0,03 alloy. The results of testing the crystal structure of the alloy Mg0,92Zn0,05C0,03 with an X-ray diffractometer showed several diffraction peaks consisting of the main phase α–Mg and a small part of the MgZn phase. Testing of Mg0,92Zn0,05C0,03 alloy after sintering with variations in temperature and 90 minutes holding time for crystal size showed that the higher the sintering temperature (425 0C to 575 0C) the crystal size value decreased significantly from 82.36 nm to 18.75 nm, and the dislocation density increased from 0.113 to 0.868 lines/mm2. For micro strain decreased from 0.015 to 0.0087. However, in the very small porosity test, the increase was from 29.8% to 31.9%. As well as for density (1.8 gr/cm3) and yield strength (274 MPa) there was no significant decrease of around 1.4%, but the synthesized Mg0,92Zn0,05C0,03 alloy fulfilled as a bone implant bio material.hhThe effect of sintering temperature on the crystal structure and physical properties of the Mg0,92Zn0,05C0,03 alloy has been studied. Magnesium-based alloys are one of the alloys that have been used in industry, the health sector, and as biodegradable materials and biomaterials. The aim of this study was to determine the effect of temperature and sintering holding time on crystal size, dislocation density, microlattice strain, and yield strength, porosity and density of Mg0,92Zn0,05C0,03 alloy. The results of testing the crystal structure of the alloy Mg0,92Zn0,05C0,03 with an X-ray diffractometer showed several diffraction peaks consisting of the main phase α–Mg and a small part of the MgZn phase. Testing of Mg0,92Zn0,05C0,03 alloy after sintering with variations in temperature and 90 minutes holding time for crystal size showed that the higher the sintering temperature (425 0C to 575 0C) the crystal size value decreased significantly from 82.36 nm to 18.75 nm, and the dislocation density increased from 0.113 to 0.868 lines/mm2. For micro strain decreased from 0.015 to 0.0087. However, in the very small porosity test, the increase was from 29.8% to 31.9%. As well as for density (1.8 gr/cm3) and yield strength (274 MPa) there was no significant decrease of around 1.4%, but the synthesized Mg0,92Zn0,05C0,03 alloy fulfilled as a bone implant bio material.