试图可视化局部氢通过钒膜的渗透

Tomoyasu FUJIMARU, Yudai KIMOTO, Shoichi SATO, Naoya MIYAUCHI, Mayu NAGAMORI, Tomoko KUSAWAKE, Akiko N. ITAKURA, Yoshihisa MATSUMOTO
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引用次数: 0

摘要

尝试用operando氢显微镜观察氢通过钒膜的渗透情况。在可视化之前,确定实验条件。引入氢的钒样品表面涂有pd - 25mol %Ag合金。同时,确定了钒样品氢可视化的最佳温度。通过优化实验条件,发现渗透氢的分布与扫描电子显微镜观察到的钒颗粒形貌有一定的相关性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Attempt to Visualize the Local Hydrogen Permeation through Vanadium Membrane
An attempt is made to visualize hydrogen permeation through vanadium membranes using operando hydrogen microscopy. Prior to visualization, experimental conditions are determined. The vanadium sample surface for hydrogen introduction is coated with Pd-25 mol%Ag alloy. Also, the optimal temperature of the vanadium sample for hydrogen visualization is determined. By optimizing the experimental conditions, some correlation was found between the distribution of permeated hydrogen and the morphology of vanadium particles observed in secondary electron image of scanning electron microscopy.
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