基于FESEM的机载粒子计数器对标准粒子的统计测量方法

Zhi-liang Gao, Q. Ji, Jian Chen, Xunbiao Zhang, Wei-hong Zhang, Junge Tan, Chenyan Wang
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引用次数: 2

摘要

清洁参数的可追溯性一直受到光散射空气粒子计数器计量界的高度重视。基于大颗粒浓度的计量方法和基于统计分析的机载颗粒计数器对小颗粒计数性能的溯源方法,试图通过计数器建立阳极氧化铝(AAO)膜上颗粒分布的坐标系统,采用空气动力学方法选择统计样本,用场发射扫描电镜(FESEM)观察这些样本在膜上的分布。对标准颗粒统计测量的不确定度进行了评价,分析了不确定度范围和关键影响因素,提出了在过程控制中提高统计精度的方法。试验结果表明,该方法对改进基于FESEM和统计分析的洁净度溯源系统理论具有重要价值。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Statistical measurement method of the standard particles through airborne particle counter based on FESEM
The traceability of cleanness parameter has received high attention from the metrology industry of light-scattering airborne particle counter. Based on the metrology method of the big particle concentration and the traceability method of airborne particle counter’s counting performance on small particle size by statistical analysis, this paper tries to build a coordinate system of the particles distribution on anodic aluminum oxide (AAO) membrane through the counter, choose the statistical samples by aerodynamics, observe these samples on membrane by field emission scanning electron microscope (FESEM), evaluate the uncertainty of measurement on standard particle statistics, analyze the uncertainty range and the key affecting factor, and put forward a method of improving statistics accuracy in process control. The test results prove that the method has important value on improvement of the theory of the cleanness traceability system based on FESEM and statistical analysis.
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