ctab模板大孔二氧化硅纳米复合膜的制备与表征

Lanfang Yao, Linlin Tian, Shuo Wang, Lin Li, Ruiqing Xu, X. Fang
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引用次数: 0

摘要

以四乙氧基硅烷(TEOS)为前驱体,表面活性剂十六烷基三甲基溴化铵(CTAB)为有机模板剂,1,3,5-三甲基苯(TMB)为有机膨胀剂,采用酸催化-凝胶两步法制备了CTAB模板化的大孔二氧化硅纳米复合膜。采用XRD、FTIR和AFM对样品进行了表征。研究发现,制备大孔材料必须控制好TMB/CTAB的摩尔比。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Preparation and characterizaion of CTAB-templated large pore silica nanocomposite films
CTAB-templated large pore silica nano-composite films were prepared by means of a two-step acid-catalyzed and solgel process using tetraethoxysilane (TEOS) as the precursor, Surfactant cetyltrimethy- ammonium bromide (CTAB) as an organic template to generate the uniformity pore structure and 1,3,5-trimethyl benzene (TMB) as organic swelling agent. The obtained samples were characterized by XRD, Fourier-transform infrared (FTIR) and Atomic Force Microscopy (AFM). We found that the TMB/CTAB mol ratio must be controlled well for producing large pore materials.
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