NaFe/sub 4/P/sub 12/纳米线的合成及生长机理

Proceedings ICT2001. 20 International Conference on Thermoelectrics (Cat. No.01TH8589) Pub Date : 2001-06-08 DOI:10.1109/ICT.2001.979907

Xiaobo Hu, Hong Liu, Ji-yang Wang, Huaidong Jiang, Shanrong Zhao, Dongming Zhang, M. Gu, M. Jiang

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引用次数: 0

摘要

采用水热还原-合金化法制备了填充方角石的NaFe/ sub4 /P/ sub12 /单晶纳米线。采用x射线衍射(XRD)、电子衍射(ED)、拉曼散射(Raman)和元素分析对产物进行了表征。采用高分辨率透射电镜(HRTEM)对纳米线的微观结构进行了研究。提出了NaFe/sub 4/P/sub 12/纳米线的生长机理。

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Synthesis and growth mechanism of NaFe/sub 4/P/sub 12/ nanowires

Filled skutterudite NaFe/sub 4/P/sub 12/ single crystal nanowires were synthesized by using a hydrothermal-reduction-alloying method. X-ray diffraction (XRD), Electron diffraction (ED), Raman scattering, as well as elemental analysis were used to characterize the product. High-resolution transmission electron microscope (HRTEM) was used to investigate the microstructure of the nanowire. A growth mechanism of NaFe/sub 4/P/sub 12/ nanowire was proposed.

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Proceedings ICT2001. 20 International Conference on Thermoelectrics (Cat. No.01TH8589)

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