静电纺丝法制备硅基氧化物荧光纳米纤维的研究

Y. Chao, Chi-Chieh Li, C. Chung
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引用次数: 0

摘要

本研究采用单轴静电纺丝法制备了硅基氧化物荧光纳米纤维。聚乙烯吡咯烷酮与醇和二甲基甲酰胺混合,以四乙氧基硅烷为硅源制备前驱体。最后,在溶液中加入硝酸钇、硝酸钙和硝酸铕进行静电纺丝,用扫描电镜观察纳米纤维的表面形貌;热重分析仪用于测量不同温度下的失重,水滴角测试仪用于测试亲疏水性。通过扫描电镜观察纳米纤维的表面形貌,纺丝时纤维的平均直径为143 nm, 600℃煅烧后纤维的平均直径为147 nm。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
A Study of Silicon-based Oxide Fluorescent Nanofibers by Electrospinning
In this study, uniaxial electrospinning was used to prepare silicon-based oxide fluorescent nanofibers. Polyvinylpyrrolidone was mixed with alcohol and dimethylformamide, and tetraethoxysilane was used as the silicon source to prepare the precursor. Finally, yttrium nitrate, calcium nitrate, and europium nitrate are added to the solution for electrospinning,Use scanning electron microscope to investigate the surface morphology of nanofibers; thermogravimetric analyzer to measure weight loss at different temperatures and water drop angle tester to test hydrophilic and hydrophobic properties. After observing the surface morphology of the nanofibers with a scanning electron microscope, the average diameter of the as-spun fibers was 143 nm and the average diameter of the fibers after calcined at 600 °C was 147 nm.
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