J. Safaei‐Ghomi, Atefeh Bakhtiari, Raheleh Teymuri
{"title":"SBA-15有机-无机杂化表面固载多相含pd催化剂的制备及其在吡啶嘧啶绿色合成中的应用","authors":"J. Safaei‐Ghomi, Atefeh Bakhtiari, Raheleh Teymuri","doi":"10.2139/SSRN.3726992","DOIUrl":null,"url":null,"abstract":"A new functionalized SBA-15 mesoporous silica has been prepared as a catalyst and characterized by different analytical techniques to determine the quality of the catalyst, including X-ray diffraction spectroscopy (XRD), Temperature Programmed Desorption (TPD), N 2 adsorption analysis, Field emission scanning electron microscopy (FE-SEM), X-Ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), Fourier-transform infrared spectroscopy (FT-IR), Energy-dispersive X-ray spectroscopy (EDX), and Thermogravimetric, Differential thermal analysis (TGA-DTA). The efficiency of the catalyst has been evaluated by synthesizing a wide range of polyfunctionalized pyrido[2,3-d] pyrimidines. This method provides several advantages containing mild reaction conditions, excellent yields in short times, the reusability of the catalyst and low catalyst loading.","PeriodicalId":314762,"journal":{"name":"ChemRN: Materials Characterization (Topic)","volume":"44 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2020-11-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Preparation of Heterogeneous Pd-Containing Catalysts Anchored on a Hybrid Organic-Inorganic Surface of SBA-15 and its Application in Green Synthesis of Pyridopyrimidines\",\"authors\":\"J. Safaei‐Ghomi, Atefeh Bakhtiari, Raheleh Teymuri\",\"doi\":\"10.2139/SSRN.3726992\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A new functionalized SBA-15 mesoporous silica has been prepared as a catalyst and characterized by different analytical techniques to determine the quality of the catalyst, including X-ray diffraction spectroscopy (XRD), Temperature Programmed Desorption (TPD), N 2 adsorption analysis, Field emission scanning electron microscopy (FE-SEM), X-Ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), Fourier-transform infrared spectroscopy (FT-IR), Energy-dispersive X-ray spectroscopy (EDX), and Thermogravimetric, Differential thermal analysis (TGA-DTA). The efficiency of the catalyst has been evaluated by synthesizing a wide range of polyfunctionalized pyrido[2,3-d] pyrimidines. This method provides several advantages containing mild reaction conditions, excellent yields in short times, the reusability of the catalyst and low catalyst loading.\",\"PeriodicalId\":314762,\"journal\":{\"name\":\"ChemRN: Materials Characterization (Topic)\",\"volume\":\"44 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2020-11-09\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"ChemRN: Materials Characterization (Topic)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2139/SSRN.3726992\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"ChemRN: Materials Characterization (Topic)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2139/SSRN.3726992","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Preparation of Heterogeneous Pd-Containing Catalysts Anchored on a Hybrid Organic-Inorganic Surface of SBA-15 and its Application in Green Synthesis of Pyridopyrimidines
A new functionalized SBA-15 mesoporous silica has been prepared as a catalyst and characterized by different analytical techniques to determine the quality of the catalyst, including X-ray diffraction spectroscopy (XRD), Temperature Programmed Desorption (TPD), N 2 adsorption analysis, Field emission scanning electron microscopy (FE-SEM), X-Ray photoelectron spectroscopy (XPS), Transmission electron microscopy (TEM), Fourier-transform infrared spectroscopy (FT-IR), Energy-dispersive X-ray spectroscopy (EDX), and Thermogravimetric, Differential thermal analysis (TGA-DTA). The efficiency of the catalyst has been evaluated by synthesizing a wide range of polyfunctionalized pyrido[2,3-d] pyrimidines. This method provides several advantages containing mild reaction conditions, excellent yields in short times, the reusability of the catalyst and low catalyst loading.