{"title":"Sb自通量法制备CoSb/sub - 3/化合物的合成及rietveld分析","authors":"T. Souma, M. Ohtaki","doi":"10.1109/ICT.2005.1519903","DOIUrl":null,"url":null,"abstract":"High purity CoSb3 bulk crystals have been successfully synthesized by Sb self-flux method and a relation between reaction conditions and chemical composition on the method has been systematically analyzed by powder XRD study using the Rietveld analysis. Sb self flux method at 923 K using 100 mesh Co elements can directly provide a single phase CoSb3 bulk crystal in a brief time of 10 h. Advantages of Sb self-flux methods will be discussed compared with other preparation methods.","PeriodicalId":422400,"journal":{"name":"ICT 2005. 24th International Conference on Thermoelectrics, 2005.","volume":"78 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2005-06-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Synthesis and rietveld analysis for CoSb/sub 3/ compounds prepared by Sb self-flux method\",\"authors\":\"T. Souma, M. Ohtaki\",\"doi\":\"10.1109/ICT.2005.1519903\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"High purity CoSb3 bulk crystals have been successfully synthesized by Sb self-flux method and a relation between reaction conditions and chemical composition on the method has been systematically analyzed by powder XRD study using the Rietveld analysis. Sb self flux method at 923 K using 100 mesh Co elements can directly provide a single phase CoSb3 bulk crystal in a brief time of 10 h. Advantages of Sb self-flux methods will be discussed compared with other preparation methods.\",\"PeriodicalId\":422400,\"journal\":{\"name\":\"ICT 2005. 24th International Conference on Thermoelectrics, 2005.\",\"volume\":\"78 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2005-06-19\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"ICT 2005. 24th International Conference on Thermoelectrics, 2005.\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/ICT.2005.1519903\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"ICT 2005. 24th International Conference on Thermoelectrics, 2005.","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/ICT.2005.1519903","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Synthesis and rietveld analysis for CoSb/sub 3/ compounds prepared by Sb self-flux method
High purity CoSb3 bulk crystals have been successfully synthesized by Sb self-flux method and a relation between reaction conditions and chemical composition on the method has been systematically analyzed by powder XRD study using the Rietveld analysis. Sb self flux method at 923 K using 100 mesh Co elements can directly provide a single phase CoSb3 bulk crystal in a brief time of 10 h. Advantages of Sb self-flux methods will be discussed compared with other preparation methods.
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