{"title":"氯三苯基{顺-1,2-双(二苯基膦基)乙烯}锡(IV)的合成和x射线晶体结构:以不明二氧二膦为例","authors":"Corrado Pelizzi, Giancarlo Pelizzi","doi":"10.1016/0020-1650(80)80026-2","DOIUrl":null,"url":null,"abstract":"<div><p>A 1:1 adduct between chlorotriphenyltin and <em>cis</em>-1,2-bis(diphenylphosphinyl)ethylene has been synthesized and characterized. The X-ray analysis has revealed a trigonal bipyramidal arrangement around tin involving three carbon atoms, the chloride ion and one of the two oxygen atoms from a unidentate phosphorus ligand.</p></div>","PeriodicalId":13630,"journal":{"name":"Inorganic and Nuclear Chemistry Letters","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"1980-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0020-1650(80)80026-2","citationCount":"18","resultStr":"{\"title\":\"Synthesis and x-ray crystal structure of chlorotriphenyl {cis-1,2-bis(diphenylphosphinyl)ethylene}tin(IV): A case of unidentate dioxo-diphosphine\",\"authors\":\"Corrado Pelizzi, Giancarlo Pelizzi\",\"doi\":\"10.1016/0020-1650(80)80026-2\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>A 1:1 adduct between chlorotriphenyltin and <em>cis</em>-1,2-bis(diphenylphosphinyl)ethylene has been synthesized and characterized. The X-ray analysis has revealed a trigonal bipyramidal arrangement around tin involving three carbon atoms, the chloride ion and one of the two oxygen atoms from a unidentate phosphorus ligand.</p></div>\",\"PeriodicalId\":13630,\"journal\":{\"name\":\"Inorganic and Nuclear Chemistry Letters\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1980-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1016/0020-1650(80)80026-2\",\"citationCount\":\"18\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Inorganic and Nuclear Chemistry Letters\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/0020165080800262\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Inorganic and Nuclear Chemistry Letters","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/0020165080800262","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Synthesis and x-ray crystal structure of chlorotriphenyl {cis-1,2-bis(diphenylphosphinyl)ethylene}tin(IV): A case of unidentate dioxo-diphosphine
A 1:1 adduct between chlorotriphenyltin and cis-1,2-bis(diphenylphosphinyl)ethylene has been synthesized and characterized. The X-ray analysis has revealed a trigonal bipyramidal arrangement around tin involving three carbon atoms, the chloride ion and one of the two oxygen atoms from a unidentate phosphorus ligand.
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