{"title":"Orientation Determination by Continuous Etching Patterns in Copper and Copper Alloys","authors":"W. Wang, X. Sun, G. Köhlhoff, K. Lücke","doi":"10.1155/TSM.24.199","DOIUrl":"https://doi.org/10.1155/TSM.24.199","url":null,"abstract":"A new method for determination of grain orientations using etch patterns was developed for copper \u0000and copper alloys. This method is based on the fact, that one gets etch patterns characteristic for the \u0000crystallographic orientation of the etched surface, if a specimen of copper or copper alloys is etched \u0000in conc. HNO3. In contrast to etch pits, the etch patterns are developed continuously over the whole \u0000grain. This allows a direct and continuous observation of the orientation changes within and between \u0000the grains, which is not possible for many other orientation determination methods. The determination \u0000accuracy of the new method depends on the crystallographic orientation of the etched surface and varies \u0000between 2° and 10°. For some special surface orientations the etch patterns allow even the determination \u0000of very small orientation changes (≤ 2°), occurring e.g. in a deformed grain.","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"132 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"122495607","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
V. Gundyrev, K. M. Demchuk, A. Martemianov, G. G. Taluts
{"title":"INFLUENCE OF POWDER STRUCTURE ON TEXTURE FORMATION IN SUPERCONDUCTING BI(PB)-SR-CA-CU-O CERAMICS IN MAGNETIC FIELD","authors":"V. Gundyrev, K. M. Demchuk, A. Martemianov, G. G. Taluts","doi":"10.1155/TSM.32.65","DOIUrl":"https://doi.org/10.1155/TSM.32.65","url":null,"abstract":"Starting powder of Bi(Pb)–Sr–Ca–Cu–O superconductor consisting mainly of 2223- \u0000phase was separated into fractions by precipitation in toluene. The high-oriented stacking \u0000of grains of the monocrystalline fractions with different dispersity has been obtained in \u0000magnetic field of 2 T at room temperature. The size of the powder grains in the range of \u00002–20 μm has no strong influence on the texture. The best result of grain alignment has \u0000been obtained for the powder grains of 10 μm in size.","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"11 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"122198116","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Neutron Depolarization in Submicron Ferromagnetic Materials","authors":"M. Rekveldt","doi":"10.1155/TSM.11.127","DOIUrl":"https://doi.org/10.1155/TSM.11.127","url":null,"abstract":"The neutron depolarization technique is based on the loss of polarization of a polarized neutron beam after transmission through ferromagnetic substances. This loss, caused by Larmor precession in individual domains, determines the mean domain size, the mean square direction cosines of the domains and the mean magnetization. The method is complementary to the neutron scattering technique with respect to the size of the inhomogeneities to be determined and the dynamic range accessible. Only the static applications of the method in studying domain structures are considered. As examples will be treated metal foils under stress, oriented ferroxdur permanent magnets, soft ferrites, recording tapes and thin films. In most of these examples magnetic correlations between neighbouring domains are subject of study.","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"26 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"117095349","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Texture Analysis of Quartz in a Granite Mylonite byEBSP-Orientation Imaging Microscopy","authors":"A. Pearson, F. Heidelbach, H. Wenk","doi":"10.1155/TSM.29.185","DOIUrl":"https://doi.org/10.1155/TSM.29.185","url":null,"abstract":"The crystallographic preferred orientation (texture) of the quartz phase in a mylonitic \u0000leucogranite from the Santa Rosa mylonite zone was investigated using automated \u0000analysis of electron backscattering patterns (EBSP) in the scanning electron microscope \u0000(SEM). The separation of the quartz diffraction patterns from patterns of other constituents \u0000(feldspar, mica, etc.) in this polymineralic rock was achieved using an image \u0000quality parameter. The quartz phase displays a texture typical for high temperature \u0000mylonites (c-axis maximum in the intermediate strain direction). The misorientation \u0000distribution between next neighbors is dominated by Dauphine twins.","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"32 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129565919","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"X-Ray Diffraction Method forDetermination of Texture Evolution inLayers","authors":"I. Tomov, R. Banova, S. Surnev","doi":"10.1155/TSM.19.189","DOIUrl":"https://doi.org/10.1155/TSM.19.189","url":null,"abstract":"An X-ray diffraction method for the determination of texture evolution in electrodeposited and \u0000vapour-deposited layers was developed. It was applied to the study of the texture of electrodeposited \u0000bright zinc. It was established that the arising of texture in the concrete models is due to oriented \u0000nucleation as well as to a growth selection process. The substrate structure also has an effect on the \u0000character of the texture evolution.","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"17 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129628270","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"TEXTURE ASYMMETRIES AS SHEAR SENSE INDICATORS IN NATURALLY DEFORMED MONO- AND POLYPHASE CARBONATE ROCKS","authors":"B. Leiss, S. Siegesmund, K. Weber","doi":"10.1155/TSM.33.61","DOIUrl":"https://doi.org/10.1155/TSM.33.61","url":null,"abstract":"The microstructural and quantitative texture analyses of a naturally deformed calcite \u0000mylonite, a dolomite mylonite and a dolomitic calcite mylonite reveal different texture \u0000asymmetries for comparable deformation conditions. Calcite shows a c-axis maximum \u0000rotated against the shear sense with regard to the main shear plane. In contrast, the \u0000dolomite shows a c-axis maximum rotated with the shear sense. In accordance with the \u0000experimental and simulated textures from the literature, this difference proves e-twinning \u0000and r-slip for calcite and f-twinning and c-slip for dolomite as the main deformation \u0000mechanisms. The dolomitic calcite mylonite shows for both the calcite and the dolomite a \u0000c-axis maximum rotated against the shear sense. On account of the microstructure of this \u0000sample, the dolomite texture has been passively overtaken from the deformation texture of \u0000calcite during a late-deformative dolomitization. The results significantly contribute to the \u0000interpretation that the sampled shear zone is a transpressive strike–slip fault.","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"5 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130396553","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"RESIDUAL STRESS AND TEXTURE DUE TO COLD AND HOT EXTRUSION PROCESSES","authors":"A. Pyzalla, W. Reimers","doi":"10.1155/TSM.33.291","DOIUrl":"https://doi.org/10.1155/TSM.33.291","url":null,"abstract":"The residual stress state and the texture of cold forward extruded full and hollow steel bodies as well as a hot extruded AlSi25Cu4Mg1 tube are studied by X-ray, high energy synchrotron and neutron diffraction. The experimental results reveal that all samples are fibre textured and that there are characteristic distributions of the residual stresses vs. sample diameter. In case of the cold forward extruded samples at low degrees of natural strain, the rod kernel is under compressive residual stresses which are balanced by tensile residual stresses in the outer part of the sample. In contrast to this, the outer part of the hot extruded sample is under compressive macroscopic stresses which are balanced by tensile macroscopic residual stresses in the inner part of the sample.","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"17 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126667723","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Editorial Comments on the Symposium on Microscale Textures ofMaterials 21-23 October 1991, Cincinnati","authors":"B. Adams, H. Weiland","doi":"10.1155/TSM.20.1","DOIUrl":"https://doi.org/10.1155/TSM.20.1","url":null,"abstract":"","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"13 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126919074","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"TEXTURE EVOLUTION IN CHANNEL-DIE COMPRESSION PART II: EFFECTS OF GRAINS WHICH SHEAR","authors":"R. Becker, L. A. Lalli","doi":"10.1155/TSM.14-18.145","DOIUrl":"https://doi.org/10.1155/TSM.14-18.145","url":null,"abstract":"resulted from slip on crystallographic planes. The model accounted for finite deformations and lattice rotations. Compatibility and equilibrium were satisfied by the finite element method. Local grain interactions produced complex deformation patterns and stress fields. The resulting crystallographic texture was compared to predictions from a Taylor type ’3 polycrystal texture evolution","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"115 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"124224872","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Tensile deformation induced texture transformation in austenitic stainless steel","authors":"S. Grigull","doi":"10.1080/07303300310001628616","DOIUrl":"https://doi.org/10.1080/07303300310001628616","url":null,"abstract":"Texture patterns of the starting ώ and transformed α structural phases were obtained from AISI 304 stainless \u0000steel sheets subjected to varying levels of tensile deformation using high energy X-ray diffraction in combination \u0000with the texture enhanced Rietveld method. The use of this method allows the simultaneous determination \u0000of the orientation distribution functions (ODF) of both phases, even for small α-martensite fractions of \u0000the order of 5%. The texture patterns are analyzed in terms of the crystallographic orientation relation \u0000between the starting and transformed phases and the preferential formation of certain variants of this relation.","PeriodicalId":129427,"journal":{"name":"Textures and Microstructures","volume":"18 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"127746490","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}