SYNTHESIS AND CHARACTERIZATION OF CALCIUM SILICATE FROM RICE HUSK ASH AND SNAIL SHELL

S. Husain, N. H. Haryanti, S. Suryajaya, Antung Permitaria
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引用次数: 6

Abstract

Calcium silicate ceramics have been made using natural ingredients such as rice husk and snail shell with solid reaction techniques. The aim of this study to determine the characteristics of calcium silicate that have been sintered at a temperature of 900 °C, 1000 °C, and 1100 °C. Samples were characterized by X-Ray Diffraction (XRD), optical microscopy, and Fourier Transform Infra-Red (FTIR). The results of XRD characterization showed that CaSiO3 (calcium silicate) along with the increase in calcination temperature and quantity was increased due to the increase of temperature of calcination. FTIR analysis showed that the Ca-Si-O bond was formed at wave number ranging from 848 cm-1 and 999 – 1001 cm-1.

稻壳灰和螺壳制备硅酸钙及其性能研究
以稻壳、螺壳等天然原料为原料,采用固相反应技术制备硅酸钙陶瓷。本研究的目的是确定在900°C, 1000°C和1100°C下烧结的硅酸钙的特性。采用x射线衍射(XRD)、光学显微镜和傅里叶变换红外(FTIR)对样品进行了表征。XRD表征结果表明,随着煅烧温度的升高,硅酸钙(CaSiO3)的含量也随着煅烧温度的升高而增加。FTIR分析表明,Ca-Si-O键在848 cm-1和999 ~ 1001 cm-1的波数范围内形成。
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