Synthesis and Characterization of Ag-Decorated TiO2 Nanoparticles for Photocatalytic Application

Q3 Materials Science
K. Balachandran, G. Vijayakumar, S. Mageswari, A. Preethi, M.S. Viswak Senan
{"title":"Synthesis and Characterization of Ag-Decorated TiO2 Nanoparticles for Photocatalytic Application","authors":"K. Balachandran, G. Vijayakumar, S. Mageswari, A. Preethi, M.S. Viswak Senan","doi":"10.13074/jent.2021.12.14446","DOIUrl":null,"url":null,"abstract":"TiO2 nanoparticles (TiO2) and Ag-doped TiO2 nanocomposites (Ag-TiO2) were synthesized by the Sol-Gel process using titanium tetra isopropoxide as TiO2 and AgNO3 as Ag precursors, respectively. The synthesized nanocomposites were characterized by XRD, SEM, TEM, FT-IR, and UV­-Visible analysis. The XRD results show that Ag doping increases the grain size from 22 nm to 36 nm. From the UV-Visible spectra, the redshift in absorbance was observed, which indicates the increase in grain size and it reduces the bandgap. The TEM analysis shows that all the particles are exhibited in the nanometer range. The synthesized nanoparticles show good photocatalytic activity, and they decompose the methyl orange dye within 5 hours.","PeriodicalId":36296,"journal":{"name":"Journal of Water and Environmental Nanotechnology","volume":"8 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-12-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Water and Environmental Nanotechnology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.13074/jent.2021.12.14446","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Materials Science","Score":null,"Total":0}
引用次数: 1

Abstract

TiO2 nanoparticles (TiO2) and Ag-doped TiO2 nanocomposites (Ag-TiO2) were synthesized by the Sol-Gel process using titanium tetra isopropoxide as TiO2 and AgNO3 as Ag precursors, respectively. The synthesized nanocomposites were characterized by XRD, SEM, TEM, FT-IR, and UV­-Visible analysis. The XRD results show that Ag doping increases the grain size from 22 nm to 36 nm. From the UV-Visible spectra, the redshift in absorbance was observed, which indicates the increase in grain size and it reduces the bandgap. The TEM analysis shows that all the particles are exhibited in the nanometer range. The synthesized nanoparticles show good photocatalytic activity, and they decompose the methyl orange dye within 5 hours.
光催化用银修饰TiO2纳米粒子的合成与表征
以四异丙醇钛为TiO2, AgNO3为Ag前驱体,采用溶胶-凝胶法制备了TiO2纳米粒子(TiO2)和Ag掺杂TiO2纳米复合材料(Ag-TiO2)。采用XRD、SEM、TEM、FT-IR和UV -可见分析对合成的纳米复合材料进行了表征。XRD结果表明,Ag的掺杂使晶粒尺寸由22 nm增大到36 nm。在紫外可见光谱上观察到吸光度的红移,表明晶粒尺寸增大,带隙减小。TEM分析表明,所制备的颗粒均在纳米级范围内。合成的纳米颗粒具有良好的光催化活性,在5小时内就能分解甲基橙染料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 求助全文
来源期刊
Journal of Water and Environmental Nanotechnology
Journal of Water and Environmental Nanotechnology Materials Science-Materials Science (miscellaneous)
CiteScore
2.40
自引率
0.00%
发文量
0
审稿时长
8 weeks
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信