Filter Preparation Techniques for Dust Exposure Determination by Gravimetric Analysis

A. Sass-Kortsak, C. Tracy, J. Purdham
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引用次数: 3

Abstract

Abstract Gravimetric analyses are frequently used to measure worker exposure to airborne particulate. In this study, two filter conditioning methods, designed to overcome moisture effects, were compared using two different filter media. Polyvinyl chloride (PVC) filters were used to sample wood dust and cork dust. Mixed cellulose ester (MCE) membrane filters were also used to sample cork dust. For each filter, pre- and postsampling weights were each determined twice: after conditioning for 48 hours in a silica gel dessicator and after being placed in an incubator set at 27°C and a nominal relative humidity of 50 percent. When MCE membrane filters were used, a statistically significant difference between conditioning methods was found in filter preweights. When PVC filters were used, weight differences between the two conditioning methods was found to be insignificant and considered potentially less important than differences due to material loss. Dessication of filters prior to weighing may result in incre...
用重量分析法测定粉尘暴露的过滤器制备技术
摘要重量分析法经常用于测量工人对空气中颗粒物的暴露。在本研究中,采用两种不同的过滤介质,比较了两种旨在克服水分影响的过滤调节方法。聚氯乙烯(PVC)过滤器用于采样木粉尘和软木粉尘。混合纤维素酯(MCE)膜过滤器也用于软木粉尘的取样。对于每个过滤器,采样前和采样后的权重分别测定两次:在硅胶干燥器中调理48小时后,以及在27°C和50%标称相对湿度的培养箱中放置后。当使用MCE膜过滤器时,不同的调节方法在过滤器预权重上有统计学上的显著差异。当使用PVC过滤器时,发现两种调节方法之间的重量差异微不足道,并且认为可能比材料损失造成的差异更重要。称重前过滤器干燥可能导致增加…
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