{"title":"Synthesis of Biocompatible ZnO/β-CD Nanocomposite and Photocatalytic Degradation Study with Methylene Blue Dye","authors":"T. Rajalakshmi, G. Alagumuthu","doi":"10.30799/JNST.S14.19050311","DOIUrl":null,"url":null,"abstract":"Article history: Received 20 March 2019 Accepted 29 April 2019 Available online 08 June 2019 In this present work zinc oxide/ β-cyclodextrin nanocomposite was successfully synthesized by a simple precipitation method using zinc nitrate hexa hydrate and sodium carbonate as precursors. The prepared ZnO nanoparticles were mixed with β-cyclodextrin solution under proper proportions and formed nanocomposite then annealed at 150 C for 2 h. The prepared samples were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), UVvisible spectroscopy and AFM. The XRD results indicate that the ZnO crystal has a hexagonal wurtzite structure. The optical properties of the samples are investigated by measuring the UV-VIS absorption at room temperature. FTIR results prove the functional groups present. Photocatalytic degradation of methylene blue (MB) dye was studied using the synthesized nanocomposites applied as photocatalyst.","PeriodicalId":23576,"journal":{"name":"Volume 5, Issue 2","volume":"1 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-07-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Volume 5, Issue 2","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30799/JNST.S14.19050311","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Article history: Received 20 March 2019 Accepted 29 April 2019 Available online 08 June 2019 In this present work zinc oxide/ β-cyclodextrin nanocomposite was successfully synthesized by a simple precipitation method using zinc nitrate hexa hydrate and sodium carbonate as precursors. The prepared ZnO nanoparticles were mixed with β-cyclodextrin solution under proper proportions and formed nanocomposite then annealed at 150 C for 2 h. The prepared samples were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), UVvisible spectroscopy and AFM. The XRD results indicate that the ZnO crystal has a hexagonal wurtzite structure. The optical properties of the samples are investigated by measuring the UV-VIS absorption at room temperature. FTIR results prove the functional groups present. Photocatalytic degradation of methylene blue (MB) dye was studied using the synthesized nanocomposites applied as photocatalyst.