[Determination of thiocyanate ions in saliva by coupling high performance liquid chromatography with specific electrode].

F Guyon, M T Couchard
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Abstract

An electrochemical method for determination of thiocyanide ions in saliva was established. The procedure involves coupling high performance liquid chromatography (HPLC) on bounded silica gel (in order to eliminate the interference of some ions) with specific electrode. This method is sensitive, precise, rapid and requires only few samples. It offers a great interest in toxicology for the detection of smoking exposure.

高效液相色谱-特定电极联用法测定唾液中硫氰酸盐离子
建立了测定唾液中硫氰化物离子的电化学方法。该方法包括在有界硅胶上耦合高效液相色谱(HPLC)(以消除某些离子的干扰)和特定电极。该方法灵敏、精确、快速,样品量少。它提供了一个很大的兴趣毒理学检测吸烟暴露。
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