N. N. Isakova, A. I. Kalyukanov, I. P. Makarova, V. T. Em
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引用次数: 0
Abstract
A methodology for measuring and taking into account the background in a single-crystal neutron experiment with a position-sensitive detector is proposed. This methodology makes it possible to increase the ratio of integrated intensities to the standard deviation I/σ(I) for diffraction reflections and thereby supplement the experimental dataset with weak reflections that previously did not meet the condition I/σ(I) > 3 and were not taken into account in crystallographic calculations. The methodology was tested on experimental data during structural studies of Cs4(HSO4)3(H2PO4) crystals on the MOND diffractometer at the IR-8 reactor of the National Research Centre “Kurchatov Institute.”
期刊介绍:
Crystallography Reports is a journal that publishes original articles short communications, and reviews on various aspects of crystallography: diffraction and scattering of X-rays, electrons, and neutrons, determination of crystal structure of inorganic and organic substances, including proteins and other biological substances; UV-VIS and IR spectroscopy; growth, imperfect structure and physical properties of crystals; thin films, liquid crystals, nanomaterials, partially disordered systems, and the methods of studies.