Stability of electron ptychography at low electron dose.

IF 1.9 4区 工程技术 Q3 MICROSCOPY
M Dearg, N Michaelides, J Gilbert, Z Ding, Z Aslam, D G Hopkinson, C S Allen, L Clark
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引用次数: 0

Abstract

Electron ptychography provides a promising avenue towards dose-efficient, high-resolution materials characterisation. Prior work demonstrates the feasibility of this approach, but an overarching view on the reliability of ptychographic images in low-dose scenarios is required. Here, we address this limitation with a systematic study of image clarity across dose, thickness and convergence semi-angle, on a range of materials science specimens. With the now widespread adoption of 4D-STEM and ptychographic imaging, the establishment of the practical parameter space in which one can anticipate a reliably interpretable phase image is urgently needed. In some cases, our parameter space exploration confirms high-resolution imaging at doses of 200  e - ${\rm e}^-$ Å - 2 $^{-2}$ .

低电子剂量下电子型图的稳定性。
电子型图为高剂量、高分辨率的材料表征提供了一条有前途的途径。先前的工作证明了这种方法的可行性,但在低剂量的情况下,需要对胸电图图像的可靠性有一个总体的看法。在这里,我们通过对一系列材料科学标本的剂量,厚度和会聚半角的图像清晰度进行系统研究来解决这一限制。随着4D-STEM和平面成像技术的广泛应用,迫切需要建立能够预测可靠可解释相位图像的实用参数空间。在某些情况下,我们的参数空间探索证实了200 e -$ {\rm e}^-$ Å -2 $^{-2}$剂量的高分辨率成像。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Journal of microscopy
Journal of microscopy 工程技术-显微镜技术
CiteScore
4.30
自引率
5.00%
发文量
83
审稿时长
1 months
期刊介绍: The Journal of Microscopy is the oldest journal dedicated to the science of microscopy and the only peer-reviewed publication of the Royal Microscopical Society. It publishes papers that report on the very latest developments in microscopy such as advances in microscopy techniques or novel areas of application. The Journal does not seek to publish routine applications of microscopy or specimen preparation even though the submission may otherwise have a high scientific merit. The scope covers research in the physical and biological sciences and covers imaging methods using light, electrons, X-rays and other radiations as well as atomic force and near field techniques. Interdisciplinary research is welcome. Papers pertaining to microscopy are also welcomed on optical theory, spectroscopy, novel specimen preparation and manipulation methods and image recording, processing and analysis including dynamic analysis of living specimens. Publication types include full papers, hot topic fast tracked communications and review articles. Authors considering submitting a review article should contact the editorial office first.
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