MicroPhotoGas Reactor: High-Throughput Experimentation for Photoinduced Reactions under a Gas Atmosphere

IF 3.1 3区化学 Q2 CHEMISTRY, APPLIED

Organic Process Research & Development Pub Date : 2025-05-19 DOI:10.1021/acs.oprd.5c00118

Sylvain Foucquart, Taline Kerackian, Géraud Chacktas, Jean-Christophe Cintrat, Eugénie Romero

引用次数: 0

Abstract

High-throughput experimentation (HTE) has transformed the exploration of many catalytic processes from a mechanistic and timeline point of view. However, some specific reactions remain impossible to transpose in HTE, mostly because of the lack of dedicated devices. With the development of photoinduced reactions involving gases as reactants, it is of importance to access HTE for such setups. We describe here the design and manufacture of a specific device for miniaturization and parallelization of photoinduced reactions under the pressure of a specific gas atmosphere.

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微光气反应器：气体环境下光诱导反应的高通量实验

高通量实验（HTE）从机制和时间的角度改变了许多催化过程的探索。然而，一些特定的反应仍然无法在HTE中转位，主要是因为缺乏专用设备。随着以气体为反应物的光致反应的发展，获得这种装置的高通量辐射是很重要的。我们在这里描述了一个特定的装置的设计和制造，用于在特定气体气氛的压力下实现光诱导反应的小型化和并行化。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

Organic Process Research & Development 化学-应用化学

CiteScore

6.90

自引率

14.70%

发文量

251

审稿时长

2 months

期刊介绍： The journal Organic Process Research & Development serves as a communication tool between industrial chemists and chemists working in universities and research institutes. As such, it reports original work from the broad field of industrial process chemistry but also presents academic results that are relevant, or potentially relevant, to industrial applications. Process chemistry is the science that enables the safe, environmentally benign and ultimately economical manufacturing of organic compounds that are required in larger amounts to help address the needs of society. Consequently, the Journal encompasses every aspect of organic chemistry, including all aspects of catalysis, synthetic methodology development and synthetic strategy exploration, but also includes aspects from analytical and solid-state chemistry and chemical engineering, such as work-up tools，process safety, or flow-chemistry. The goal of development and optimization of chemical reactions and processes is their transfer to a larger scale; original work describing such studies and the actual implementation on scale is highly relevant to the journal. However, studies on new developments from either industry, research institutes or academia that have not yet been demonstrated on scale, but where an industrial utility can be expected and where the study has addressed important prerequisites for a scale-up and has given confidence into the reliability and practicality of the chemistry, also serve the mission of OPR&D as a communication tool between the different contributors to the field.