L. O. Kozlova, I. L. Voroshilov, Yu. V. Ioni, Yu. D. Ivakin, I. V. Kozerozhets, M. G. Vasiliev
{"title":"Low-temperature Synthesis of Highly Dispersed Barium Aluminate","authors":"L. O. Kozlova, I. L. Voroshilov, Yu. V. Ioni, Yu. D. Ivakin, I. V. Kozerozhets, M. G. Vasiliev","doi":"10.1134/S0036023624602071","DOIUrl":null,"url":null,"abstract":"<p>A new approach for the low-temperature synthesis of highly dispersed barium aluminate of vermicular morphology with specified characteristics (bulk density from 0.015 g/cm<sup>3</sup>, average particle size in the range of 15–87 nm) has been developed. The synthesis technique includes sequential heat treatment of a concentrated aqueous solution of BaCl<sub>2</sub>, Al(NO<sub>3</sub>)<sub>3</sub>, (NH<sub>2</sub>)<sub>2</sub>CO, and C<sub>6</sub>H<sub>8</sub>O<sub>7</sub> up to 1200°C. Using physicochemical research methods, including IR spectroscopy, X-ray powder diffraction, transmission and scanning electron microscopy, as well as chemical analysis, the main stages of the synthesis of BaAl<sub>2</sub>O<sub>4</sub> are characterized.</p>","PeriodicalId":762,"journal":{"name":"Russian Journal of Inorganic Chemistry","volume":"69 11","pages":"1619 - 1625"},"PeriodicalIF":1.8000,"publicationDate":"2024-11-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of Inorganic Chemistry","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S0036023624602071","RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CHEMISTRY, INORGANIC & NUCLEAR","Score":null,"Total":0}
引用次数: 0
Abstract
A new approach for the low-temperature synthesis of highly dispersed barium aluminate of vermicular morphology with specified characteristics (bulk density from 0.015 g/cm3, average particle size in the range of 15–87 nm) has been developed. The synthesis technique includes sequential heat treatment of a concentrated aqueous solution of BaCl2, Al(NO3)3, (NH2)2CO, and C6H8O7 up to 1200°C. Using physicochemical research methods, including IR spectroscopy, X-ray powder diffraction, transmission and scanning electron microscopy, as well as chemical analysis, the main stages of the synthesis of BaAl2O4 are characterized.
期刊介绍:
Russian Journal of Inorganic Chemistry is a monthly periodical that covers the following topics of research: the synthesis and properties of inorganic compounds, coordination compounds, physicochemical analysis of inorganic systems, theoretical inorganic chemistry, physical methods of investigation, chemistry of solutions, inorganic materials, and nanomaterials.