Low-temperature Synthesis of Highly Dispersed Barium Aluminate

IF 1.8 3区 化学 Q3 CHEMISTRY, INORGANIC & NUCLEAR
L. O. Kozlova, I. L. Voroshilov, Yu. V. Ioni, Yu. D. Ivakin, I. V. Kozerozhets, M. G. Vasiliev
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引用次数: 0

Abstract

A new approach for the low-temperature synthesis of highly dispersed barium aluminate of vermicular morphology with specified characteristics (bulk density from 0.015 g/cm3, average particle size in the range of 15–87 nm) has been developed. The synthesis technique includes sequential heat treatment of a concentrated aqueous solution of BaCl2, Al(NO3)3, (NH2)2CO, and C6H8O7 up to 1200°C. Using physicochemical research methods, including IR spectroscopy, X-ray powder diffraction, transmission and scanning electron microscopy, as well as chemical analysis, the main stages of the synthesis of BaAl2O4 are characterized.

Abstract Image

低温合成高分散铝酸钡
本文提出了一种低温合成高分散铝酸钡的新方法,该方法具有特定的蠕虫状形貌(体积密度为0.015 g/cm3,平均粒径为15 ~ 87 nm)。该合成技术包括将BaCl2、Al(NO3)3、(NH2)2CO和C6H8O7的浓水溶液依次热处理至1200℃。利用红外光谱、x射线粉末衍射、透射电镜和扫描电镜等理化研究方法,以及化学分析,对BaAl2O4合成的主要阶段进行了表征。
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来源期刊
Russian Journal of Inorganic Chemistry
Russian Journal of Inorganic Chemistry 化学-无机化学与核化学
CiteScore
3.10
自引率
38.10%
发文量
237
审稿时长
3 months
期刊介绍: Russian Journal of Inorganic Chemistry is a monthly periodical that covers the following topics of research: the synthesis and properties of inorganic compounds, coordination compounds, physicochemical analysis of inorganic systems, theoretical inorganic chemistry, physical methods of investigation, chemistry of solutions, inorganic materials, and nanomaterials.
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