Ethanol-assisted in situ stimulated graphene oxide as support for CuO/NiO nanoparticles†

IF 3.9 3区 化学 Q2 CHEMISTRY, MULTIDISCIPLINARY
RSC Advances Pub Date : 2024-11-25 DOI:10.1039/D4RA04308A
Manash J. Baruah, Eramoni Saikia, Nand Kishor Gour, N. Priyanshu Singh, Bitupon Borthakur, Uttam Mohan, Arup Jyoti Das, Rahul Kemprai, Bikash K. Sarmah, Rupjyoti Dutta, Young-Bin Park, Biraj Das and Mukesh Sharma
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引用次数: 0

Abstract

Herein we report the first successful synthesis of ethanol-assisted in situ generated reduced graphene oxide as a support for CuO/NiO nanoparticles. Through the strategic incorporation of Cu and Ni precursors into ethanol, followed by thermal treatment, we achieved the fabrication of reduced graphene oxide-supported CuO/NiO nanoparticles. The material underwent thorough characterization using FT-IR, XRD, TEM, XPS, Raman, and UV-DRS analysis. This method promises a breakthrough approach unveiling an unparalleled potential leading to paradigm shifts in graphene oxide synthesis. A theoretical study has also been performed in support of GO formation from ethanol. The synthesized CuO/NiO nanoparticles over reduced graphene oxide were found to be effective for the reduction of 4-nitrophenol within 5 min.

Abstract Image

乙醇辅助原位激发氧化石墨烯作为 CuO/NiO 纳米粒子的支撑†。
在此,我们首次成功合成了乙醇辅助原位生成的还原氧化石墨烯,作为 CuO/NiO 纳米粒子的支撑物。通过在乙醇中策略性地加入铜和镍前驱体,然后进行热处理,我们制备出了还原氧化石墨烯支撑的 CuO/NiO 纳米粒子。我们使用 FT-IR、XRD、TEM、XPS、拉曼和 UV-DRS 分析对材料进行了全面的表征。这种方法有望成为一种突破性的方法,揭示出无与伦比的潜力,引领氧化石墨烯合成的范式转变。此外,还进行了一项理论研究,以支持从乙醇中形成 GO。研究发现,在还原氧化石墨烯上合成的 CuO/NiO 纳米粒子可在 5 分钟内有效还原 4-硝基苯酚。
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来源期刊
RSC Advances
RSC Advances chemical sciences-
CiteScore
7.50
自引率
2.60%
发文量
3116
审稿时长
1.6 months
期刊介绍: An international, peer-reviewed journal covering all of the chemical sciences, including multidisciplinary and emerging areas. RSC Advances is a gold open access journal allowing researchers free access to research articles, and offering an affordable open access publishing option for authors around the world.
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