Recent Progress and Applications of Advanced Nanomaterials in Solid-Phase Extraction.

IF 3 3区生物学 Q2 BIOCHEMICAL RESEARCH METHODS

ELECTROPHORESIS Pub Date : 2024-11-05 DOI:10.1002/elps.202400152

Pin Chen, Qiuyue Zhang, Hang Yin, Siyuan Di, Huan Liu, Hailan Qin, Ming Liu, Yunkang Liu, Zihan Li, Shukui Zhu

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引用次数: 0

Abstract

Sample preparation maintains a key bottleneck in the whole analytical procedure. Solid-phase sorbents (SPSs) have garnered increasing attention in sample preparation research due to their crucial roles in achieving high clean-up and enrichment efficiency in the analysis of trace targets present in complex matrices. Novel nanoscale materials with improved characteristics have garnered considerable interest across different scientific disciplines due to the limited capabilities of traditional bulk-scale materials. The purpose of this review is to offer a thorough summary of the latest developments and uses of SPSs in preparing samples for chromatographic analysis, focusing on the years 2020-2024. The techniques for preparing SPSs are examined, such as metal-organic frameworks (MOFs), covalent organic frameworks (COFs), carbon nanoparticles (CNPs), molecularly imprinted polymers (MIPs), and metallic nanomaterials (MNs). Examining the pros and cons of different extraction methods, including solid-phase extraction (SPE), magnetic SPE (MSPE), flow-based SPE (FBA-SPE), solid-phase microextraction (SPME), stir-bar sorptive extraction (SBSE), and dispersive SPE (DSPE), is the main focus. Furthermore, this article presents the utilization of SPE technology for isolating common contaminants in various environmental, biological, and food specimens. We highlight the persistent challenges in SPSs and anticipate future advancements and applications of novel SPSs.

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先进纳米材料在固相萃取中的最新进展和应用。

样品制备是整个分析过程中的关键瓶颈。固相吸附剂（SPSs）在分析复杂基质中的痕量目标物时，在实现高净化和高富集效率方面发挥着至关重要的作用，因此在样品制备研究中受到越来越多的关注。由于传统大体积材料的能力有限，具有更佳特性的新型纳米材料在不同科学学科中都引起了极大的兴趣。本综述旨在全面总结 SPS 在制备色谱分析样品方面的最新发展和应用，重点关注 2020-2024 年。本综述探讨了制备 SPS 的技术，如金属有机框架 (MOF)、共价有机框架 (COF)、碳纳米颗粒 (CNP)、分子印迹聚合物 (MIP) 和金属纳米材料 (MN)。本文的重点是研究不同萃取方法的优缺点，包括固相萃取（SPE）、磁性固相萃取（MSPE）、流式固相萃取（FBA-SPE）、固相微萃取（SPME）、搅拌棒吸附萃取（SBSE）和分散固相萃取（DSPE）。此外，本文还介绍了如何利用固相萃取技术分离各种环境、生物和食品样本中的常见污染物。我们强调了固相萃取技术长期面临的挑战，并对新型固相萃取技术的未来发展和应用进行了展望。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

ELECTROPHORESIS 生物-分析化学

CiteScore

6.30

自引率

13.80%

发文量

244

审稿时长

1.9 months

期刊介绍： ELECTROPHORESIS is an international journal that publishes original manuscripts on all aspects of electrophoresis, and liquid phase separations (e.g., HPLC, micro- and nano-LC, UHPLC, micro- and nano-fluidics, liquid-phase micro-extractions, etc.). Topics include new or improved analytical and preparative methods, sample preparation, development of theory, and innovative applications of electrophoretic and liquid phase separations methods in the study of nucleic acids, proteins, carbohydrates natural products, pharmaceuticals, food analysis, environmental species and other compounds of importance to the life sciences. Papers in the areas of microfluidics and proteomics, which are not limited to electrophoresis-based methods, will also be accepted for publication. Contributions focused on hyphenated and omics techniques are also of interest. Proteomics is within the scope, if related to its fundamentals and new technical approaches. Proteomics applications are only considered in particular cases. Papers describing the application of standard electrophoretic methods will not be considered. Papers on nanoanalysis intended for publication in ELECTROPHORESIS should focus on one or more of the following topics: • Nanoscale electrokinetics and phenomena related to electric double layer and/or confinement in nano-sized geometry • Single cell and subcellular analysis • Nanosensors and ultrasensitive detection aspects (e.g., involving quantum dots, "nanoelectrodes" or nanospray MS) • Nanoscale/nanopore DNA sequencing (next generation sequencing) • Micro- and nanoscale sample preparation • Nanoparticles and cells analyses by dielectrophoresis • Separation-based analysis using nanoparticles, nanotubes and nanowires.