Development of molecularly imprinted polymer-based dispersive micro-solid-phase extraction for the selective extraction of histamine from canned tuna fish samples prior to its determination by GC–FID

IF 2.2 4区 化学 Q2 Engineering
Sanaz Kamrani, Mohammad Reza Afshar Mogaddam, Mir Ali Farajzadeh, Mahboob Nemati, Aramdokht Khatibi
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引用次数: 0

Abstract

A molecularly imprinted polymer-based dispersive micro-solid-phase extraction method has been developed for the efficient extraction and preconcentration of histamine from tuna fish samples prior to its determination by gas chromatography–flame ionization detector. In this approach, a molecularly imprinted polymer was prepared by chemical oxidation of pyrrole using iron (III) chloride, and then, it was characterized by Fourier transform infrared spectroscopy and scanning electron microscopy and used in the extraction procedure. The method was validated using the International Council Research Protocol, and the results showed low limits of detection (0.06 mg kg−1) and quantification (0.21 mg kg−1), good precision (relative standard deviation = 3.2%), linearity (r2 ≥ 0.9969) and acceptable extraction recovery (98%). The method was successfully done on various tuna fish samples, and histamine was determined in them.

开发基于分子印迹聚合物的分散微固相萃取技术,用于选择性萃取金枪鱼罐头样品中的组胺,然后利用气相色谱-质谱联用仪进行测定
研究人员开发了一种基于分子印迹聚合物的分散微固相萃取方法,用于在气相色谱-火焰离子化检测器测定金枪鱼样品中的组胺之前对其进行高效萃取和预浓缩。在该方法中,利用氯化铁(III)对吡咯进行化学氧化制备了分子印迹聚合物,然后利用傅里叶变换红外光谱和扫描电子显微镜对其进行了表征,并将其用于萃取过程。结果表明,该方法的检出限(0.06 mg kg-1)和定量限(0.21 mg kg-1)均较低,精密度(相对标准偏差 = 3.2%)、线性关系(r2 ≥ 0.9969)和萃取回收率(98%)均可接受。该方法成功地用于多种金枪鱼样品中组胺的测定。
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来源期刊
Chemical Papers
Chemical Papers Chemical Engineering-General Chemical Engineering
CiteScore
3.30
自引率
4.50%
发文量
590
期刊介绍: Chemical Papers is a peer-reviewed, international journal devoted to basic and applied chemical research. It has a broad scope covering the chemical sciences, but favors interdisciplinary research and studies that bring chemistry together with other disciplines.
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