Microstructures and Mechanical Properties of 12Cr12Mo Martensitic Stainless Steel Manufactured by Selective Laser Melting

IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
Runqi Yang, Linzhi Wang, Yikai Xiong, Chenyu Liao, Ting Li
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Abstract

In this study, 12Cr12Mo martensitic stainless steel was manufactured using selective laser melting (SLM). The resulting microstructures and mechanical properties were analyzed under optimal process parameters to understand the correlation between the process, microstructure, and properties. The results showed that only a single martensitic phase is present in the SLM samples, attributed to the exceptionally rapid solidification rate and high density of dislocations. It was observed that the 12Cr12Mo microstructure consists of interspersed columnar and equiaxed grains at the microscale, while fine body-centered cubic (bcc) lath martensite with high dislocation density is observed at the submicron scale. SLM-prepared 12Cr12Mo stainless steel exhibits impressive mechanical properties due to its hierarchical microstructure. Under optimal process parameters, the fabricated samples achieved a microhardness of 544.91 HV, with yield and ultimate tensile strengths of 729 ± 24 and 842 ± 19 MPa, respectively, but elongation is limited to 7 ± 0.6%. The cellular and martensitic structures with high dislocation density along grain boundaries are the mean factor for the increased strength but reduced ductility. Observations of a disintegrated surface and river-like patterns suggest a brittle fracture mode in 12Cr12Mo stainless steel prepared by SLM.

Abstract Image

选择性激光熔融法制造的 12Cr12Mo 马氏体不锈钢的微观结构和力学性能
本研究采用选择性激光熔融(SLM)技术制造了 12Cr12Mo 马氏体不锈钢。在最佳工艺参数条件下,对所获得的微观结构和机械性能进行了分析,以了解工艺、微观结构和性能之间的相关性。结果表明,SLM 样品中只存在单一的马氏体相,这归因于极快的凝固速度和高密度的位错。据观察,12Cr12Mo 的微观结构在微观尺度上由穿插的柱状和等轴晶粒组成,而在亚微米尺度上则观察到具有高位错密度的细小体心立方(bcc)板条马氏体。SLM 制备的 12Cr12Mo 不锈钢因其层次分明的微观结构而表现出令人印象深刻的机械性能。在最佳工艺参数下,制备的样品达到了 544.91 HV 的显微硬度,屈服强度和极限抗拉强度分别为 729 ± 24 MPa 和 842 ± 19 MPa,但伸长率限制在 7 ± 0.6%。沿晶界具有高位错密度的蜂窝状和马氏体结构是强度提高但延展性降低的主要因素。通过观察崩解表面和河流状图案,可以看出 SLM 制备的 12Cr12Mo 不锈钢具有脆性断裂模式。
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来源期刊
Journal of Materials Engineering and Performance
Journal of Materials Engineering and Performance 工程技术-材料科学:综合
CiteScore
3.90
自引率
13.00%
发文量
1120
审稿时长
4.9 months
期刊介绍: ASM International''s Journal of Materials Engineering and Performance focuses on solving day-to-day engineering challenges, particularly those involving components for larger systems. The journal presents a clear understanding of relationships between materials selection, processing, applications and performance. The Journal of Materials Engineering covers all aspects of materials selection, design, processing, characterization and evaluation, including how to improve materials properties through processes and process control of casting, forming, heat treating, surface modification and coating, and fabrication. Testing and characterization (including mechanical and physical tests, NDE, metallography, failure analysis, corrosion resistance, chemical analysis, surface characterization, and microanalysis of surfaces, features and fractures), and industrial performance measurement are also covered
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