Performance Evaluation of Multiple Aging-Regeneration of SBS-Modified Bitumen Regenerated by a Composite Rejuvenator

Song Xu, Bingtao Xu, Shishui Liulin, Shaoxu Cai, Guangming Tang, Shilong Pan
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Abstract

In this study, compound regeneration of SBS-modified bitumen (SMB) was carried out by a composite rejuvenator composed of furfural extraction oil (FEO) and 1,6-hexanediol diglycidyl ether (HDDGE) in the presence of catalyst triethanolamine (TEOA). SMB was subjected to three aging-regeneration cycles, and the physical and rheological properties, toughness and tenacity, and chemical structures of the SMB after each aging-regeneration cycle were tested to investigate the regeneration effect of the composite rejuvenator on SMB at different numbers of cycles. The ductility decreases and low-temperature properties deteriorate as the number of cycles increased, but the high-temperature properties of the SMB are improved. The complex modulus aging index and phase angle aging index indicate that the viscous behavior of SMB weakens after the second and third aging. The degree of viscoelasticity and toughness recovery decreases with the increase in the number of cycles, and the tenacity of SMB after the third aging-regeneration cycle is basically lost. The results of the Fourier transform infrared (FTIR) spectra tests prove that with the increase in the aging–regeneration cycles of SMB, the intensity of FTIR peaks of oxygen-containing functional groups is greater, and the recovery of aged SMB is gradually weakened.
复合再生器再生 SBS 改性沥青的多重老化-再生性能评估
本研究在催化剂三乙醇胺(TEOA)存在的条件下,采用由糠醛提取油(FEO)和1,6-己二醇二缩水甘油醚(HDDGE)组成的复合再生剂对SBS改性沥青(SMB)进行了复合再生。对 SMB 进行了三次老化再生循环,测试了每个老化再生循环后 SMB 的物理流变性能、韧性和韧性以及化学结构,以研究复合再生剂在不同循环次数下对 SMB 的再生效果。随着循环次数的增加,SMB 的延展性下降,低温性能恶化,但高温性能得到改善。复合模量老化指数和相角老化指数表明,SMB 的粘性行为在第二次和第三次老化后会减弱。粘弹性和韧性的恢复程度随着循环次数的增加而降低,SMB 在第三次老化-再生循环后韧性基本丧失。傅立叶变换红外光谱(FTIR)测试结果证明,随着 SMB 老化再生周期的增加,含氧官能团的 FTIR 峰强度增大,老化 SMB 的恢复能力逐渐减弱。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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