Emulsified Epoxy Resin for Mitigating Sand Production

F. F. Chang, F. Liang, Christie Lee, Paul Berger
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Abstract

Sand production from unconsolidated or crushed weakly consolidated formations due to high reservoir fluid flow velocity leads to operational problems and limits their potential. Many techniques are practiced by the completion and production engineers to combat such challenge. This paper discusses the development and testing of a novel polymeric resin formulation that consolidates sand grains to form a high regained permeability and high compressive strength rock matrix, allowing high production rate without sanding concern. The new chemical solution utilizes a low viscosity water external epoxy emulsion to strengthens the bonding of sand grains while maintains flow capacity. The chemical formulation contains two components that can be batch mixed at wellsite, injected by coiled tubing or drill pipe, and shut-in in the formation to cure for 24 to 48 hours depending on the reservoir temperature from 200°F to 320°F. Unlike most of the currently used resin consolidation products, by which post flush is required to maintain opening of the pore space, the emulsion separates during the curing process with epoxy attaching to the sand surface while the water phase occupies the pore to help keep the flow path open. Laboratory experiments in both water or oil saturated sand packs showed the treated loose sand are well consolidated with the unconfined compressive strength significantly greater than 1000 psi and the regained permeability up to 54%. No sand production was observed in the produced fluid at high flow rates. This paper focuses on the laboratory testing of the water external emulsified epoxy. The chemical mechanism and evaluation methodology are described. Having the water emulsified epoxy resin system allows the convention water based diverting techniques such as foam to be used during treatment of long sections. Another benefit of the water based emulsified epoxy is its operation simplicity and safety. The flash point concerns for safe field operation is completely alleviated with this chemical formulation.
用于减少产砂的乳化环氧树脂
由于储层流体流速较高,从未固结或破碎的弱固结地层中产砂会导致作业问题,并限制其潜力。完井和生产工程师采用了许多技术来应对这种挑战。本文讨论了一种新型聚合物树脂配方的开发和测试,该配方可固结砂粒,形成高渗透率和高抗压强度的岩石基质,从而实现高生产率,且无需担心砂化问题。新的化学解决方案利用一种低粘度水外环氧乳液来加强砂粒的粘合,同时保持流动能力。该化学配方包含两种成分,可在井场批量混合,通过盘管或钻杆注入,并根据储层温度(200°F 至 320°F)在地层中固化 24 至 48 小时。目前使用的大多数树脂固结产品都需要后期冲洗来保持孔隙的开放,而乳液则不同,它在固化过程中会分离,环氧树脂会附着在砂表面,而水相则占据孔隙,帮助保持流道的开放。在含水或含油饱和砂组中进行的实验室实验表明,经过处理的松散砂粒固结良好,无压抗压强度明显大于 1000 psi,渗透率恢复到 54%。在高流速条件下,生产流体中未观察到产砂现象。本文重点介绍水外乳化环氧的实验室测试。介绍了化学机制和评估方法。水乳化环氧树脂系统允许在处理长断面时使用传统的水基分流技术,如泡沫。水基乳化环氧树脂的另一个优点是操作简单、安全。有了这种化学配方,对现场安全操作闪点的担忧就完全没有了。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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