Investigations of Crystal Structure and Magnetic Properties of Mn0.3Fe2.7O4/PEO/PMMA/AC Nanocomposites

A. S. H. Wahyuni, S. Sunaryono, N. M. Chusna, H. Wisodo, Anugrah Pratama Supriyono, N. Mufti, A. Taufiq
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Abstract

The Mn0.3Fe2.7O4/PEO/PMMA/AC nanocomposites were synthesized using co-precipitation and solid-state reaction methods. The Mn0.3Fe2.7O4/PEO/PMMA/AC nanocomposites were success formed. This was confirmed by characterization using FTIR instrument. The Fe-O, C-O, and C-H2 functional groups were the representation of Mn0.3Fe2.7O4, PEO/PMMA, and AC respectively. Investigation of crystal structure was characterized using XRD instrument. According to X-Ray Diffraction analysis, the crystal size was 10.82 nanometers and the peak of AC was detected on 2θ around 24.85o. In addition, the investigation of magnetic properties was characterized using VSM instrument. This result showed that the Mn0.3Fe2.7O4/PEO/PMMA/AC nanocomposites behave as a superparamagnetic material with a saturation magnetization value was around 12.55 emu/gram.
Mn0.3Fe2.7O4/PEO/PMMA/AC 纳米复合材料的晶体结构和磁性能研究
采用共沉淀法和固相反应法合成了Mn0.3Fe2.7O4/PEO/PMMA/AC纳米复合材料。成功地形成了 Mn0.3Fe2.7O4/PEO/PMMA/AC 纳米复合材料。傅立叶变换红外光谱仪的表征证实了这一点。Mn0.3Fe2.7O4、PEO/PMMA 和 AC 分别代表了 Fe-O、C-O 和 C-H2 官能团。利用 XRD 仪器对晶体结构进行了表征。根据 X 射线衍射分析,晶体尺寸为 10.82 纳米,AC 的峰值在 2θ 24.85o 左右。此外,还使用 VSM 仪器对磁性能进行了表征。结果表明,Mn0.3Fe2.7O4/PEO/PMMA/AC 纳米复合材料是一种超顺磁性材料,其饱和磁化值约为 12.55 埃姆/克。
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