Synthesis and single crystal X-ray studies of bis-(trimethylsilylmethyl) tellurium diiodide through an insertion route

IF 1.3 4区 化学 Q3 CHEMISTRY, MULTIDISCIPLINARY
Amit K. Tripathi, Priyanka Singh, Ray J. Butcher, J. Bera, Puspendra Singh
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引用次数: 0

Abstract

 The synthesis and single crystal X-ray studies of bis(trimethylsilylmethyl) telluriumdiiodide was studied through an insertion route with quantitative yield. This molecule was characterized with the help of 1H NMR, elemental analysis and single-crystal X-ray studies. The new crystalline molecule provides a supramolecular synthon in crystal lattices of tellurium(IV) diiodide showing 2d synthons associated with the help of C-H - - - I interactions.
通过插入路线合成双-(三甲基硅甲基)二碘化碲并进行单晶 X 射线研究
通过插入路线研究了双(三甲基硅甲基)二碘化碲的合成和单晶 X 射线研究,并获得了定量收率。借助 1H NMR、元素分析和单晶 X 射线研究对该分子进行了表征。这种新的晶体分子在二碘化碲(IV)晶格中提供了一种超分子合成物,在 C-H - - I 相互作用的帮助下显示出 2d 合成物。
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来源期刊
Main Group Chemistry
Main Group Chemistry 化学-化学综合
CiteScore
2.00
自引率
26.70%
发文量
65
审稿时长
>12 weeks
期刊介绍: Main Group Chemistry is intended to be a primary resource for all chemistry, engineering, biological, and materials researchers in both academia and in industry with an interest in the elements from the groups 1, 2, 12–18, lanthanides and actinides. The journal is committed to maintaining a high standard for its publications. This will be ensured by a rigorous peer-review process with most articles being reviewed by at least one editorial board member. Additionally, all manuscripts will be proofread and corrected by a dedicated copy editor located at the University of Kentucky.
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