N,N′-Dipropyloxamide

IF 0.6 Q4 CHEMISTRY, ORGANIC

Molbank Pub Date : 2023-12-22 DOI:10.3390/m1753

E. Podda, Eleanor Dodd, M. Arca, M. Aragoni, Vito Lippolis, S. Coles, Anna Pintus

引用次数: 0

Abstract

N,N′-Dipropyloxamide (1) was synthesised by the reaction between diethyloxalate and n-propylamine in ethanol. Compound 1 was fully characterised by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by the slow evaporation of a methyl alcohol solution of the compound. The resulting crystal structure shows the prominent role exerted by intermolecular hydrogen bonds in the crystal packing.

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产品名称

N,N′-Dipropyloxamide (1) 是通过二乙氧基丙酸盐和正丙胺在乙醇中的反应合成的。通过微量分析（元素分析、熔点测定）和光谱分析（傅立叶变换红外光谱和核磁共振光谱）对化合物 1 进行了全面鉴定。通过缓慢蒸发化合物的甲醇溶液，分离出了适合进行单晶 X 射线衍射的晶体。由此得到的晶体结构表明，分子间氢键在晶体堆积中发挥了重要作用。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

Molbank Chemistry-Physical and Theoretical Chemistry

CiteScore

0.70

自引率

33.30%

发文量

174

审稿时长

11 weeks

期刊介绍： •organic synthesis •biosynthesis •extraction and purification •natural product derivatives •structural elucidation (X-ray crystallography, NMR, etc.)