{"title":"Zeolite-Based Silica Synthesis With Calcination Temperature Variations 100oC, 150oC and 200oC","authors":"Helisa Duwi Maesari, Misfalakhul Hidayah","doi":"10.21580/jnsmr.2018.4.2.11019","DOIUrl":null,"url":null,"abstract":"This research on Zeolite-Based Silica Synthesis with Calcination Temperature Variations 100 , 150 , and 200 . The purpose of this study was to determine the effect of calcination temperature on the silica structure contained in zeolites. Synthesis is made from zeolite, NaOH and HCl by sol-gel method and temperature calcination treatment 100 , 150 , and 200 . Zeolite samples were characterized by XRD (X- Ray Diffraction). The results showed that sample A with temperature 100 contains Quartz silica, moganite silica (SiO2), and Aluminum Oxide (Al2O3). Sample B with temperature 150 contains Quartz silica (SiO2), and Anorthite (AlCaO8Si). Sample C with 200 contains Quartz silica and Aluminium Oxide (Al2O3). As for the crystallite size in sample A measuring 678.51 nm, sample B measuring 488.16 nm and sample C measuring 488.13 nm. ©2018 JNSMR UIN Walisongo. All rights reserved.","PeriodicalId":191192,"journal":{"name":"Journal of Natural Sciences and Mathematics Research","volume":"9 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2018-12-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Natural Sciences and Mathematics Research","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.21580/jnsmr.2018.4.2.11019","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
煅烧温度100oC, 150oC和200oC下沸石基二氧化硅的合成
研究了沸石基二氧化硅在煅烧温度100、150和200下的合成。本研究的目的是确定煅烧温度对沸石中二氧化硅结构的影响。以沸石、NaOH和HCl为原料,经100、150、200的温度煅烧处理,采用溶胶-凝胶法合成。采用XRD (X射线衍射)对沸石样品进行了表征。结果表明,温度为100℃的样品A中含有石英、二氧化硅和氧化铝(Al2O3)。样品B温度为150,含有石英二氧化硅(SiO2)和钙长石(AlCaO8Si)。样品C含有石英、二氧化硅和氧化铝(Al2O3)。样品A的晶粒尺寸为678.51 nm,样品B的晶粒尺寸为488.16 nm,样品C的晶粒尺寸为488.13 nm。©2018 JNSMR UIN Walisongo。版权所有。
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