SINTESIS DAN KARAKTERISASI NANOPARTIKEL Fe2O3 DARI PASIR ALAM DESA LOGAS KABUPATEN KUANTAN SINGINGI

Abstract

Determination of magnetic and structural properties of natural sand from Logas Village, Kuantan Singingi have been carried out using a magnetic Probe Pasco PS-2162 and X-Ray Diffraction methode. Samples were synthesized using multi step ball milling methode for 90 and 90+30 hours. Results show that the magneticsuceptibility increased with increasing of ball milling time, from 90 hours to 90+30 hours. This magnetic suceptibility within the interval (46-80000) x 10-8 m3/kg which is the interval of Ilminite mineral (FeTiO3; Antiferromagnetic). X-Ray Fluorescence result showed that the composition of Fe and Ti increased after milled for 90+30 hours, while other element like Si decreased. The XRD result confirmed that the phase of the sample structure is Hematite (α-Fe2O3). However, some other phases including SiO2 and FeTiO3 are observed in diffraction pattern. This indicates that the sample is not purely hematite.