Modification and Characterization of Polyamide Nanocomposites with Organobentonite Cetyltrimethylammonium Bromide

Barita Aritonang, A. H. Ritonga, Karnirius Harefa
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Abstract

Modification of bentonite with Cetyl Trimethyl Ammonium Bromide (CTAB) has been successfully carried out, resulting in the application of organobentonite as a filler. The purpose of this study was to determine the characteristics of the polyamide nanocomposite material before and after the addition of organobentonite filler. Commercial bentonite after being modified with CTAB is organophilic with a particle size of 9.55 nm. The results of the Fourier Transform Infra Red spectrum analysis show that there is a wide and sharp absorption band at wave number 3749.6 cm-1 which indicates the presence of Al-OH groups. The results of Scanning Electron Microscopy analysis of the surface morphology of the polyamide/organobentonite nanocomposite obtained a homogeneous and compatible mixture. The conclusion from the CTAB research results can unite polyamide and bentonite which have different polarities
十六烷基三甲基溴化铵有机膨润土对聚酰胺纳米复合材料的改性及表征
采用十六烷基三甲基溴化铵(CTAB)对膨润土进行了改性,实现了有机膨润土作为填料的应用。本研究的目的是测定添加有机膨润土填料前后聚酰胺纳米复合材料的性能。经CTAB改性后的膨润土为亲有机膨润土,粒径为9.55 nm。傅里叶变换红外光谱分析结果表明,在波数为3749.6 cm-1处存在一个宽而锐利的吸收带,表明Al-OH基团的存在。扫描电镜分析了聚酰胺/有机膨润土纳米复合材料的表面形貌,得到了均匀相容的混合物。CTAB的研究结果可以将极性不同的聚酰胺和膨润土结合起来
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